Pavement thermoregulation paving material based on phase-change heat accumulation microcapsules
A phase-change heat storage material and road surface temperature technology, applied in building insulation materials, building components, buildings, etc., can solve problems such as unusable and cost constraints, and achieve the effects of prolonging service life, reducing temperature sensitivity, and high strength
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Embodiment 1
[0030] A pavement temperature regulating pavement material based on phase change heat storage microcapsule technology, obtained by the following method:
[0031] Add 57 parts (mass, the same below) of petroleum asphalt (origin: Shanjiasi) heated to 90-140°C into the reactor, add 1.14 parts of maleimide, raise the temperature to 130-135°C, and wait for the pressure to stabilize. Access to N 2 , keep the total pressure at 0.25MPa, and after 4 hours of reaction, slowly release the pressure to 0.1MPa. Then gradually lower the temperature to 100-110°C, add 24 parts of triethylenetetramine, then programmatically raise the temperature to 130-135°C for 1-3 hours. Then add Jingchuan 9650, 16.2 parts, 5 parts of naphthenic rubber oil, which has been heated to 90-140°C in advance, and pre-mix for 30 minutes; then disperse at high speed through a colloid mill to obtain part A, and finally add part B at a ratio of 2.0:1 Epoxy resin (E-51, Wuxi Resin Factory, wherein the quality of microc...
Embodiment 2
[0033] A pavement temperature regulating pavement material based on phase change heat storage microcapsule technology, obtained by the following method:
[0034] Add 57 parts (mass, the same below) of petroleum asphalt (origin: Shanjiasi) heated to 90-140°C into the reactor, add 1.14 parts of maleimide, raise the temperature to 130-135°C, and wait for the pressure to stabilize. Access to N 2 , keep the total pressure at 0.25MPa, and after 4 hours of reaction, slowly release the pressure to 0.1MPa. Then gradually lower the temperature to 100-110°C, add 14.0 parts of hexamethylenediamine, then programmatically raise the temperature to 130-135°C for 1-3 hours. Then add Jingchuan 9650, 20.2 parts, and 8 parts of furfural oil extracted in advance to 90-140 °C, and pre-mix for 30 minutes; then disperse at high speed through a colloid mill to obtain part A, and finally add part B epoxy at a ratio of 4.2:1 Resin (E-51, Wuxi Resin Factory, wherein the quality of microcapsules: the qu...
Embodiment 3
[0036] Add 57 parts (mass, the same below) of petroleum asphalt (origin: Shanjiasi) heated to 90-140°C into the reactor, add 1.14 parts of maleimide, raise the temperature to 130-135°C, and wait for the pressure to stabilize. Access to N 2, keep the total pressure at 0.25MPa, and after 4 hours of reaction, slowly release the pressure to 0.1MPa. Then gradually lower the temperature to 100-110°C, add 13.2 parts of diphenyldiaminooctadiene, and then programmatically raise the temperature to 130-135°C for 1-3 hours. Then add Jingchuan 9650, 21.5 parts, 5 parts of phenolic residue oil, which was pre-heated to 90-140 ° C, and pre-mix for 30 minutes; then disperse at high speed through a colloid mill to obtain part A, and finally add part B epoxy at a ratio of 6.8:1 Resin (E-44, Wuxi Resin Factory, wherein the quality of microcapsules: quality of epoxy resin = 20:80 and the core material of microcapsules is 1:1 ethylene glycol and OP-10) was mixed evenly. This material can be used ...
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