Method for coproduction of pistacia chinensis bunge essential oil and polyphenol
A technology of wood essential oil and Pistacia chinensis, which is applied in the field of joint production of Pistacia chinensis essential oil and polyphenols, can solve problems affecting farmers' planting enthusiasm, achieve the effect of improving comprehensive utilization value, improving economic and social benefits, and promoting development
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Embodiment 1
[0020] This embodiment includes the following steps:
[0021] (1) After drying 10kg of fresh Pistacia chinensis leaves naturally, use supercritical CO 2 The essential oil of Pistacia chinensis was extracted by the fluid extraction method, the extraction pressure was 50MPA, the extraction time was 5 hours, and the temperature was 70°C to obtain 30g of essential oil, which was a yellow transparent oily liquid.
[0022] (2) After crushing the residues of Pistacia chinensis tissue extracted from the essential oil, sieve it, add it into methanol with a mass percentage concentration of 80% according to the solid-liquid ratio of 1:200g / ml, and extract it in a water bath at 95°C for 200min; at the same time, use Ultrasonic wave 10000W is used for auxiliary extraction; after the extract is filtered out, the methanol in the solution is removed by rotary evaporation, and the crude polyphenol extract is obtained by vacuum freeze-drying.
[0023] In this example, the yield of polyphenols ...
Embodiment 2
[0025] This embodiment includes the following steps:
[0026] (1) After drying 10kg of fresh Pistacia chinensis leaves naturally, use supercritical CO 2 The essential oil of Pistacia chinensis was extracted by the fluid extraction method, the extraction pressure was 10MPA, the extraction time was 1 hour, and the temperature was 30°C to obtain 20g of the essential oil, which was a yellow transparent oily liquid.
[0027] (2) After crushing the residues of Pistacia chinensis tissue extracted from the essential oil, sieve it, add it into propanol with a mass percentage concentration of 50% according to the solid-liquid ratio of 1:2g / ml, and extract it in a water bath at 20°C for 10 minutes; at the same time Ultrasonic wave 800W is used for auxiliary extraction; then, after filtering the extract, rotary evaporation removes propanol in the solution, and vacuum freeze-drying to obtain crude polyphenol extract.
[0028] In this example, the yield of polyphenols determined by the Fol...
Embodiment 3
[0030] This embodiment includes the following steps:
[0031] (1) After drying 10kg of fresh Pistacia chinensis leaves naturally, use supercritical CO 2 The essential oil of Pistacia chinensis was extracted by the fluid extraction method, the extraction pressure was 15MPA, the extraction time was 3 hours, and the temperature was 50°C to obtain 28g of essential oil, which was a yellow transparent oily liquid.
[0032] (2) Crush the pistachio chinensis tissue residue extracted from the essential oil, sieve it, add it into ethyl acetate with a mass percentage concentration of 60% according to the solid-liquid ratio of 1:50g / ml, and extract it in a water bath at 30°C for 20 minutes; At the same time, ultrasonic wave 100W is used for auxiliary extraction; after centrifugation to separate the extract solution, ethyl acetate in the solution is removed by rotary evaporation, and the crude polyphenol extract is obtained by vacuum freeze-drying.
[0033] In this example, the yield of p...
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