Branch well bay wall solidifying liquid and preparation method thereof
A technology of solidified fluid and branched wells, applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve problems such as easy instability of the wellbore, poor compaction diagenesis, loss of branched wellbore effects, etc., to achieve Guaranteed stability, high compressive strength, and the effect of safe construction
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Embodiment 1
[0029] Embodiment 1, preparation solidification liquid
[0030] (1) Preparation of modified epoxy furan resin
[0031] Pre-dissolve epoxy furan resin with a mixed solvent composed of n-butanol and ethylene glycol butyl ether (mass ratio 1:1), ensure that it is placed in a four-neck flask equipped with a stirrer, constant pressure funnel, condenser tube and nitrogen conduit , raised the temperature to 105°C, added 1 / 2 of the total amount of BPO (benzoyl peroxide) in acetone solution (the mass concentration of BPO was 10%), and reacted for 30 minutes; AMPS (2-acrylamido-2-methyl Propanesulfonic acid) was dissolved in water, slowly added dropwise into the four-necked bottle within 1 hour, and kept warm for 30 minutes, during which time, the remaining BPO solution was added twice, and the reaction was continued for 1.0 hour. After the reaction, a light yellow transparent viscous solution is obtained, which is the AMPS modified epoxy furan resin solution, and the modified epoxy fu...
Embodiment 2
[0035] Embodiment 2, preparation solidification liquid
[0036] (1) Preparation of modified epoxy furan resin
[0037] The preparation method of the modified epoxy furan resin is the same as step (1) in Example 1.
[0038] (2) Preparation of solidified liquid
[0039] Get 10 grams of above-mentioned modified epoxy furan resins prepared and add in the beaker, take by weighing 15 grams of laurylamine and add in the beaker and mix with the modified epoxy furan resins, add 75g mass concentration in the mixed product under stirring condition. 30% sodium chloride aqueous solution, stirred at 2000 rpm for 10 minutes, is the solidified solution.
[0040] The "sand filling injection method" was used to evaluate the solidified liquid system in the example.
[0041] (1) The viscosity of the solidified liquid in Example 1 was investigated as a function of temperature and time. The results showed that the solidified liquid prepared in Example 1 had a long-term stability at room temperat...
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