Degumming method of silk
A silk degumming and silk technology, applied in the field of silk degumming, can solve the problems of inability to remove grease impurities, difficult to adjust, affecting fiber quality processing, etc., so as to improve physical and mechanical strength, reduce elongation loss at break, and reduce loss of breaking strength. Effect
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Embodiment 1
[0017] Take 5g of silk and tie it with polyester thread, place it in 0.05g / L anhydrous Na 2 CO 3 In the solution, heat it to 90-100°C in an electric thermostatic furnace, keep it warm for 2 hours, then adjust the pH value of the solution to 9 with ammonia water, apply ultrasonic waves to the solution at 70-80°C, the power of the ultrasonic waves is 400W, and the frequency is 40kHz. Ultrasonic time is 90 minutes; then, it is washed with deionized water, and the washed silk is dried to obtain degummed silk. The drying temperature is 80-90° C. and the drying time is 2 hours. The breaking strength, breaking elongation and breaking elongation of silk were measured by YG(B)001A electronic single fiber strength machine. After calculation, the breaking strength loss of silk was 28.32cN, the breaking elongation loss rate was 26.28%, and the degumming rate was 28.32cN. was 85.3%.
Embodiment 2
[0019] Take 5g of silk and tie it with polyester thread, place it in 0.05g / L anhydrous Na 2 CO 3 In the solution, heat it to 90-100°C in an electric constant temperature furnace, keep it warm for 3 hours, then adjust the pH value of the solution to 11 with ammonia water, apply ultrasonic waves to the solution at 70-80°C, the power of the ultrasonic waves is 400W, and the frequency is 40kHz. Ultrasonic time is 120 minutes; then, it is washed with deionized water, and the washed silk is dried to obtain degummed silk. The drying temperature is 80-90° C. and the drying time is 1 hour. The breaking strength, breaking elongation and breaking elongation of silk were measured by YG(B)001A electronic single fiber strength machine. After calculation, the loss of silk breaking strength after degumming was 26.93cN, the loss rate of breaking elongation was 27.54%, and the degumming rate was 86.8%.
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