Method for preparing dense fine-grain neodymium iron boron sintering magnet
A sintered magnet, NdFeB technology, applied in the direction of magnetic objects, inductor/transformer/magnet manufacturing, magnetic materials, etc., can solve the problems of reducing density and orientation, inconsistent performance, uneven shrinkage, etc., to achieve uniform shrinkage performance , The effect of simple operation and easy industrial production
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Embodiment 1
[0022] Example 1: The preparation of a Nd29.5Fe68.7Cu0.8B1.0 (wt%) sintered magnet with an average grain size of 5.8 μm and a density of 99.3% should be completed according to the following steps:
[0023] 1. Nd29.5Fe68.7Cu0.8B1.0 (wt%) alloy was cast into ingot by scales and then hydrogen broken and jet milled to obtain powder particles with an average size of 3 μm, which was oriented and pressed under a 1.8T oriented magnetic field, and 20kg oriented Put the compact into the sintering furnace, vacuumize until the vacuum degree in the furnace reaches 0.1Pa, stop vacuuming, and pass 0.3MPa high-purity argon gas into the furnace to wash the furnace;
[0024] 2. Restart vacuuming until the vacuum degree in the furnace is lower than 0.1Pa again, start heating the furnace and continue vacuuming. First, it takes 30 minutes to raise the furnace from room temperature to 300°C, and then it takes 80 minutes to raise the furnace from 300°C to 600°C, then raise the furnace from 600°C to ...
Embodiment 2
[0030] Example 2: The preparation of a Nd29.5Fe68.7Cu0.8B1.0 (wt%) sintered magnet with an average grain size of 5.2 μm and a density of 99.5% should be completed according to the following steps:
[0031] 1. Nd29.5Fe68.7Cu0.8B1.0 (wt%) alloy was cast into ingot by scales and hydrogen broken and jet milled to obtain powder particles with an average size of 3 μm, which was oriented and pressed under a 1.8T oriented magnetic field, and 20kg oriented Put the compact into the sintering furnace, vacuumize until the vacuum degree in the furnace reaches 0.1Pa, stop vacuuming, and pass 0.3MPa high-purity argon gas into the furnace to wash the furnace;
[0032] 2. Restart vacuuming until the vacuum degree in the furnace is lower than 0.1Pa again, start heating the furnace and continue vacuuming. First, it takes 30 minutes to raise the furnace from room temperature to 300°C, and then it takes 80 minutes to raise the furnace from 300°C to 600°C, then raise the furnace from 600°C to 850°C...
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