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Deep dehydration technique of Vc two-step fermentation ultrafiltration waste slag liquid

A two-step fermentation and deep dehydration technology, which is applied in the direction of ultrafiltration, can solve the problems of increased difficulty in processing or utilization, little increase in ultrafiltration speed, and difficulty in concentration, so as to improve equipment utilization and shorten ultrafiltration cycle Effect

Inactive Publication Date: 2014-01-15
SHENYANG AGRI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, after adding water, the colloidal properties of the tail liquid also changed, and the ultrafiltration speed was not greatly improved, and the area used was 400m 2 The membrane supercharges the 60 tons of tail liquid to the remaining 30-35 tons of filtrate, which takes 6-8 hours
At this time, the 30-35 tons of residual liquid can no longer be ultra-filtered, and it is called ultra-filtered waste liquid, which is directly discharged. Its water content is greater than 95%, and it is a fluid liquid with high viscosity. It is difficult to concentrate again. or use increased difficulty

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0008] Take 100ml of the ultrafiltration tail liquid whose slag concentration is 4.8g / 100ml and gulong acid concentration is 91mg / ml, adjust the pH to 2.5 with hydrochloric acid, put it into 80 after standing for 20 minutes o In a C water bath, keep warm for 20 minutes, cool to room temperature, and centrifuge at 1500 rpm for 10 minutes to remove 71ml of clear liquid containing 87mg / ml of acid and transfer it to subsequent ion exchange processes; The content is 55%. Centrifuge and dry to make feed protein.

Embodiment 2

[0010] Take 100ml of the ultrafiltration tail liquid with a concentration of 4.1g / 100ml of slag and a concentration of 96mg / ml of gulonic acid, adjust the pH to 3.5 with gulonic acid, and place it in a 70 o In a C water bath, keep warm for 30 minutes, cool to room temperature, and centrifuge at 1500 rpm for 15 minutes to remove 76ml of clear liquid containing 93mg / ml of acid and transfer it to the subsequent process; %. Centrifuge and dry to make feed protein.

Embodiment 3

[0012] Get the ultrafiltration tail liquid 300000ml that the slag concentration is 4.4g / 100ml, the gulong acid concentration is 89mg / ml, adjust pH 3.0 with sulfuric acid, import steam after standing for 20 minutes and make it heat up to 74 o C, keep warm for 30 minutes, cool to room temperature, centrifuge with a decanter centrifuge, 4800 rpm for 10 minutes, separate 230 000ml, and the clear liquid with an acid content of 84mg / ml is transferred to the subsequent process; the centrifugal precipitation is a thick sauce-like sediment, The water content is 84%, and the protein content is 50%.

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PUM

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Abstract

The invention discloses a deep dehydration technique of Vc two-step fermentation ultrafiltration waste slag liquid. Ultrafiltration raffinate with 3-5 g / 100ml of contained slag concentration and 70-120 mg / ml of gulonic acid concentration is used for regulating pH within 2-4, is stood for 20 minutes, is heated to 70-90 DEG C for keeping 20-30 minutes, is cooled to the room temperature, and is centrifugated for 10-15 minutes with 1500 rpm; supernate is shifted into originally ultrafiltered filtrate and participated in following techniques with the same; precipitate is centrifuged to form cake-shaped sediment, has 80%-84% of water content, and is dried to prepare feed protein; the protein content is 35%-55%. The deep dehydration technique is adopted to reduce 75% of emission of the ultrafiltration waste slag liquid; the water content of the ultrafiltration waste slag liquid is decreased from 95% to 80%, so that the preparation of the feed protein is guaranteed; the deep dehydration technique can shorten 30% of an ultrafiltration period, and can improve equipment utilization rate by 20%.

Description

technical field [0001] The invention relates to a deep dehydration technology of Vc two-step fermentation ultrafiltration waste liquid, specifically a process for fully concentrating the ultrafiltration waste liquid by adjusting the operating conditions in the final stage of ultrafiltration. Background technique [0002] According to the current production process of Vc two-step fermentation and ultrafiltration dehydration, the Vc fermentation mash needs to be ultrafiltered out of gulong acid with an ultrafiltration membrane with a molecular weight cut-off of 3 to 100,000 Daltons. The initial speed of ultrafiltration is very fast, with an area of ​​1500m 2 When 300 tons of mash is ultrafiltered by an ultrafiltration membrane with a molecular weight cut-off of 100,000 Daltons, 270 tons can be filtered out in 4 to 5 hours. However, as the amount of bacteria and residues accumulated in the ultrafiltration increases, the filtration rate gradually slows down. When the ultrafiltr...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D61/14
Inventor 吕淑霞陈宏权胡昊曹桂环杨伟超韩利涛刘红心张良王天晓张喆张忠泽徐慧
Owner SHENYANG AGRI UNIV
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