A liver-type fatty acid-binding protein content detection kit and preparation method thereof
A fatty acid binding and detection kit technology, applied in biological testing, measuring devices, material inspection products, etc., can solve the problems of long detection time, large manual operation impact, low degree of automation, etc., to achieve good sensitivity, ensure stability, The effect of improving specificity
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Embodiment 1
[0035] Preparation of Latex Particle Solution Coated with Hepatic Fatty Acid Binding Protein Antibody:
[0036] (1) Preparation of carboxylated modified polystyrene latex solution
[0037] Take 0.5 mL of 10% polystyrene latex particles with a particle size of 200 nm (purchased from PolyMicrospheres) in a 50 mL centrifuge tube, and add 4.5 mL of 0.12 mol / L pH7.4 phosphate (PBS) buffer to the centrifuge tube , to obtain latex microspheres by centrifugation, wash the latex microspheres twice with deionized water, and then resuspend the latex microspheres with 5 mL of phosphate (PBS) buffer with a concentration of 0.12mol / LpH7.4; Add 1.0 mL of 0.02 mol / L 6-aminocaproic acid solution to the spherical particle solution, then add 2 mg of 1-ethyl-3-(3-dimethylaminopropyl) carbodiimide (EDC), at room temperature Stir the reaction for 30 minutes, centrifuge and pour off the supernatant to make carboxylated polystyrene latex microspheres with glycine groups, and add 5 mL of phosphate (P...
Embodiment 2
[0052] Preparation of Latex Particle Solution Coated with Hepatic Fatty Acid Binding Protein Antibody:
[0053] (1) Preparation of carboxylated modified polystyrene latex solution
[0054] Take 0.5 mL of 10% polystyrene latex particles with a particle size of 200 nm (purchased from PolyMicrospheres) in a 50 mL centrifuge tube, and add 4.5 mL of 0.12 mol / L pH7.4 phosphate (PBS) buffer to the centrifuge tube , to obtain latex microspheres by centrifugation, wash the latex microspheres twice with deionized water, and then resuspend the latex microspheres with 5 mL of phosphate (PBS) buffer with a concentration of 0.12mol / LpH7.4; Add 1.0 mL of 0.02 mol / L 6-aminocaproic acid solution to the spherical particle solution, then add 2 mg of 1-ethyl-3-(3-dimethylaminopropyl) carbodiimide (EDC), at room temperature Stir the reaction for 30 minutes, centrifuge and pour off the supernatant to make carboxylated polystyrene latex microspheres with glycine groups, and add 5 mL of phosphate (P...
Embodiment 3
[0069] Preparation of Latex Particle Solution Coated with Hepatic Fatty Acid Binding Protein Antibody:
[0070] (1) Preparation of carboxylated modified polystyrene latex solution
[0071] Take 0.4 mL of 10% polystyrene latex particles with a particle size of 220 nm (purchased from PolyMicrospheres) in a 50 mL centrifuge tube, and add 4.6 mL of 0.12 mol / L pH7.4 phosphate (PBS) buffer to the centrifuge tube , to obtain latex microspheres by centrifugation, wash the latex microspheres twice with deionized water, and then resuspend the latex microspheres with 5 mL of phosphate (PBS) buffer with a concentration of 0.12mol / LpH7.4; Add 0.8 mL of 0.02 mol / L 6-aminocaproic acid solution to the spherical particle solution, then add 1.8 mg of 1-ethyl-3-(3-dimethylaminopropyl) carbodiimide (EDC), at room temperature Stir and react for 40 minutes, centrifuge and pour off the supernatant to make carboxylated polystyrene latex microspheres with aminoacetic acid groups, and buffer with 5 mL...
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