Solder composition and printed wiring board using the same
A technology of composition and solder, which is applied in the direction of printed circuits, printed circuits, welding/cutting media/materials, etc. connected with non-printed electrical components, can solve problems such as easy edge collapse and rise in preheating temperature, and achieve suppression The effect of sagging and maintaining printability
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[0051] Next, although an Example and a comparative example demonstrate this invention in more detail, this invention is not limited to these examples at all. In addition, the materials used in the Example and the comparative example are as follows.
[0052] Rosin-based resin: hydrogenated rosin, manufactured by Arakawa Chemical Industry Co., Ltd.
[0053] Solvent: Diethylene glycol monohexyl ether (DEH), manufactured by Nippon Emulsifier Co., Ltd.
[0054] Dispersion of amide-based condensate microparticles: referring to the following Production Example 1, the concentration of amide-based condensate microparticles in the dispersion is 20% by mass
[0055] Thixotropic agent A: fatty acid amide, trade name "SLIPACKS LA", manufactured by Nippon Chemicals Co., Ltd.
[0056] Thixotropic agent B: fatty acid amide, trade name "SLIPACKS H", manufactured by Nippon Chemicals Co., Ltd.
[0057] Thixotropic agent C: 12-hydroxystearic acid triglyceride, manufactured by Nippon Chemicals ...
manufacture example 1
[0064] 600.0 parts by mass of 12-hydroxystearic acid derived from hydrogenated castor oil fatty acid was added to a reaction device equipped with a stirrer, a thermometer, and a water separator, and heated to 80 to 100° C. to melt. Then, 116.0 parts by mass of hexamethylenediamine was added as a diamine, and condensation reaction was carried out while dehydrating for 5 to 8 hours at 170° C. under a nitrogen atmosphere to amidate it to obtain a product with an acid value of 4.2 and an amine value of 9.4. Low molecular weight diamide compound. Further add 68.0 parts by mass of a carboxyl group-containing polymer, which is a propylene-maleic anhydride copolymer with a weight average molecular weight of 10,000 and an acid value of 80 mg KOH / g, and condenses while dehydrating at 170° C. for 1 to 2 hours In the reaction, a part of the low-molecular-weight diamide compound is reacted with an unreacted amino group for amidation, and a high-molecular-weight diamide compound is produced...
Embodiment 1
[0067] 100 parts by mass of rosin resin, 51 parts by mass of solvent, 6.3 parts by mass of a dispersion of amide condensate particles, 1.8 parts by mass of activator A, 4.5 parts by mass of activator B, 1.2 parts by mass of Activator C and 0.4 parts by mass of an amine compound were mixed using a grinder to obtain a flux.
[0068] Then, 11% by mass of the obtained flux and 89% by mass of lead-free solder powder (100% by mass in total) were put into a container and mixed for 2 hours with a kneader to prepare a solder composition.
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