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Method for measuring and calculating drift angle and deflection of single crystal plane

A technology of single crystal crystal and crystal face, which is applied in the field of directional detection and processing of single crystal materials, achieving the effects of low cost, crystal saving and wide application

Inactive Publication Date: 2014-02-19
CHANGCHUN UNIV OF SCI & TECH
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AI Technical Summary

Problems solved by technology

[0005] In order to solve the problem that the existing X-ray crystal orientation instrument needs to repeatedly orient the crystal at off-angles, and at the same time, get rid of the existing dependence on the ideal crystal plane and crystal orientation distribution map of the measured crystal and expensive equipment by the Laue photographic method, We have invented a single crystal plane off-angle and deflection calculation method

Method used

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  • Method for measuring and calculating drift angle and deflection of single crystal plane
  • Method for measuring and calculating drift angle and deflection of single crystal plane
  • Method for measuring and calculating drift angle and deflection of single crystal plane

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Embodiment Construction

[0018] Below in conjunction with example further illustrate the method of the present invention, as shown in the accompanying drawing.

[0019] The crystal to be cut is germanium single crystal, and the ideal crystal plane for cutting is (111) crystal plane.

[0020] The step of realizing one-time directional cutting according to the method of the present invention is as follows:

[0021] (a) First roughly cut according to the crystal orientation to obtain the crystal plane to be measured, that is, according to the directional cutting of the germanium single crystal (111) crystal plane to be cut and processed, the resulting cutting plane is the crystal plane to be measured, and the crystal plane to be measured There is an off angle and a deflection between the germanium single crystal (111) crystal plane to be cut and processed, and the germanium single crystal (111) crystal plane to be cut and processed is an ideal crystal plane, and its diffraction angle θ 0 =13°39', which ...

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Abstract

The invention discloses a method for measuring and calculating a drift angle and deflection of a single crystal plane, and belongs to the technical field of oriented detection on a single crystal material. The prior art needs repeated drift angle orientation on crystals. The method comprises the following steps of 1, measuring diffraction angles of any three points on the same plane of a crystal plane to be measured by an X-ray crystal orientation instrument and marking positions of the measured three points, 2, joining the three points to form a triangle, measuring length of sides of the triangle and calculating interior angles, 3, building a space rectangular coordinate system, 4, building an equation set of known quantity and unknown quantity based on the space rectangular coordinate system, calculating coordinates of the three points and their projection points, and calculating normal vectors of the crystal plane to be measured and an ideal crystal plane, 5, calculating a drift angle of the measured crystal plane relatively to the ideal crystal plane according to a crystal system crystal-plane included-angle formula, and calculating deflection of the measured crystal plane relatively to the ideal crystal plane according to a space two-direction vector included-angle formula, and 6, adjusting a crystal cutting direction according to the drift angle and the deflection, and carrying out one-step cutting to obtain a crystal plane according with crystal orientation.

Description

technical field [0001] The invention relates to a method for measuring and calculating the declination angle and deflection of a single crystal plane. Based on an ordinary X-ray crystal orientation instrument, the declination angle and deflection of a single crystal plane are measured and calculated, belonging to the technical field of orientation detection and processing of single crystal materials. Background technique [0002] Single crystal materials have anisotropic characteristics, and optical components made of them have important applications in the field of optics. The blank for processing optical elements of single crystal material is a grown single crystal bar. After rough cutting, any crystal plane is accurately oriented and then fine cut. The accurate orientation detection of any crystal plane is called crystal orientation. For the actual processing of single crystal materials, crystal orientation is usually to measure the relationship between different parts of...

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Application Information

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IPC IPC(8): G01N23/207
Inventor 石广丰史国权胡明亮
Owner CHANGCHUN UNIV OF SCI & TECH
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