Comprehensive extraction method of rhizoma polygonati total saponins and polygahatous polysaccharides
A technology for the comprehensive extraction of Polygonatum polysaccharides, applied in the field of comprehensive extraction of Polygonatum saponins and Polygonatum polysaccharides, can solve the problems of complex procedures, high operating costs, and unfavorable industrial production, and achieve the effects of simple equipment, fewer procedures, and low production costs
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Embodiment 1
[0021] The comprehensive extraction method of Polygonatum total saponins and Polygonatum polysaccharides in this embodiment includes the extraction method of Polygonatum total saponins and the extraction method of Polygonatum polysaccharides;
[0022] 1, first carry out the extraction of Polygonatum total saponins according to the following steps:
[0023] a. Soak Polygonatum powder in ethanol with a volume concentration of 75% for 4 hours, then reflux in a constant temperature water bath at 50°C for 2 hours, and filter with suction to obtain Polygonatum extract and Polygonatum medicinal residue; For the second ethanol extraction, the Polygonatum extract obtained by merging two extractions is carried out in step b; wherein the quality of Polygonatum powder and the volume ratio of ethanol with a volume concentration of 75% are 1g:10ml;
[0024] B, the Polygonatum extract obtained in step a is concentrated under reduced pressure to obtain a concentrated solution; the concentrate...
Embodiment 2
[0031] The comprehensive extraction method of Polygonatum total saponins and Polygonatum polysaccharides in this embodiment includes the extraction method of Polygonatum total saponins and the extraction method of Polygonatum polysaccharides;
[0032] 1, first carry out the extraction of Polygonatum total saponins according to the following steps:
[0033] a. Soak Polygonatum powder in ethanol with a volume concentration of 85% for 4.5 hours, then reflux in a constant temperature water bath at 60°C for 1 hour, and filter with suction to obtain Polygonatum extract and Rhizoma Polygonatum dregs; wherein the mass and volume concentration of Polygonatum powder The volume ratio of 85% ethanol is 1g:20ml; Polygonatum herb residues are extracted with ethanol for the second time in the same way, and the Polygonatum extract obtained by merging two extractions is carried out in step b;
[0034] B, the Polygonatum extract obtained in step a is concentrated under reduced pressure to obtai...
Embodiment 3
[0041] The comprehensive extraction method of Polygonatum total saponins and Polygonatum polysaccharides in this embodiment includes the extraction method of Polygonatum total saponins and the extraction method of Polygonatum polysaccharides;
[0042] 1, first carry out the extraction of Polygonatum total saponins according to the following steps:
[0043] a. Soak Polygonatum powder in ethanol with a volume concentration of 80% for 5 hours, then reflux in a constant temperature water bath at 55°C for 1.5 hours, and filter with suction to obtain Polygonatum extract and Rhizoma Rhizoma Polygonatum; For the second ethanol extraction, the Polygonatum extract obtained by merging two extractions is carried out in step b; wherein the quality of Polygonatum powder and the volume ratio of ethanol with a volume concentration of 80% are 1g:15ml;
[0044] B, the Polygonatum extract obtained in step a is concentrated under reduced pressure to obtain a concentrated solution; the concentrated ...
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