Regeneration method for catalyst for preparing epoxypropane by propylene epoxidation
A catalyst and epoxidation technology, applied in the direction of catalyst regeneration/reactivation, metal/metal oxide/metal hydroxide catalyst, physical/chemical process catalyst, etc., can solve problems such as complex operation and difference in catalytic performance
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Embodiment 1
[0061] The fresh 0.1% Au / TS-1 catalyst was loaded in a fixed-bed reactor, the catalyst filling amount was 0.15g, and the evaluation was conducted according to conventional conditions. The deactivated catalyst was regenerated after a period of time: the reaction gas was switched to air, the temperature was raised to 300 degrees at a rate of 5 degrees per minute, and the catalyst was regenerated for 3 hours. See attached for regeneration results Figure 1-3 .
[0062] The results show that the regeneration method proposed by the present invention can effectively restore the catalytic performance of the catalyst.
Embodiment 2
[0064] Load fresh 0.15% Au / TS-1 catalyst in a fixed-bed reactor with a catalyst filling amount of 0.15g, and evaluate it according to conventional conditions. Regenerate the deactivated catalyst after a period of time: switch the reactant gas to hydrogen: oxygen: nitrogen = 0.1:1.9:8, heat up to 300 degrees at a rate of 10 degrees per minute, and regenerate the catalyst for 2 hours. See attached for regeneration results image 3 .
[0065] The results show that the regeneration method proposed by the present invention can effectively restore the catalytic performance of the catalyst.
Embodiment 3
[0067] The fresh 0.10% Au / TS-1-1-butyl-3-methylimidazole tetrafluoroborate catalyst was loaded into the fixed bed reactor, the catalyst filling amount was 0.15g, and the evaluation was carried out according to conventional conditions. Regenerate the deactivated catalyst after a period of time: switch the reaction gas to oxygen: argon=2:8, heat up to 280 degrees at a rate of 5 degrees / min, and regenerate the catalyst for 2.5 hours. See attached for regeneration results Picture 10 .
[0068] The results show that regeneration of the catalyst containing the promoter by the method proposed by the present invention can also effectively restore the catalytic performance of the catalyst.
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