A kind of air-drying unsaturated polyester resin and its production method
A polyester resin and a production method technology, applied in the field of air-drying unsaturated polyester resin and its production, can solve the problems of poor air-drying, difficult to control, low amount of paraffin wax, etc., achieve convenient polishing, increase transparency, The effect of improving air dryness
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Embodiment 1
[0034] Embodiment 1 Take the production of air-drying unsaturated polyester resin with 3600 liters of reactor as an example
[0035] raw material
[0036] Reaction feed A
[0037]
[0038] Cooling, dilution step feeding B
[0039]
[0040] production steps
[0041] 1. Check equipment, pipelines, electrical appliances, instruments, and check the type and quantity of raw materials.
[0042] 2. Put the reaction materials A into the reaction kettle: glycol, dibasic acid (anhydride), triphenyl phosphite and QS-20, etc. Heat up, 10 degrees / hour, stir after 0.5 hours, when the material heats up When the temperature reaches 120°C, start the reaction stirrer and supply 4M nitrogen 3 / h and continue to heat up the reaction.
[0043] 3. When the temperature of the distillation head rises to 98-100°C, the vertical condenser is supplied with water, the temperature of the distillation head is controlled at 100-102°C, and the reaction is kept for 1 hour after the water is discharg...
Embodiment 2
[0061] Embodiment 2 Take the production of air-drying unsaturated polyester resin with 3600 liters of reactor as an example
[0062] raw material
[0063] Reaction feed A
[0064]
[0065] Cooling, dilution step feeding B
[0066]
[0067] production steps
[0068] 1. Check equipment, pipelines, electrical appliances, instruments, and check the type and quantity of raw materials.
[0069] 2. Put the reaction materials A into the reaction kettle: glycol, dibasic acid (anhydride), triphenyl phosphite and QS-20, etc. Heat up, stir after 0.5 hours, 10 degrees / hour, when the material heats up When the temperature reaches 120°C, start the reaction stirrer and supply 4M nitrogen 3 / h and continue to heat up the reaction.
[0070] 3. When the temperature of the distillation head rises to 98-100°C, the vertical condenser is supplied with water, the temperature of the distillation head is controlled at 100-102°C, and the reaction is kept for 1 hour after the water is discharged...
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Abstract
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