Liquid solid magnetic separation method
A technology of magnetic separation and magnetic separator, which is applied in the field of magnetic separation of Fischer-Tropsch synthesis heavy products and solid catalysts in a slurry bed, can solve the problems that fine particle catalysts are not easy to settle and carry out a lot of catalysts, and achieve continuous long-term cycle. Operational, easy to implement, efficient separation effect
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Embodiment 1-4
[0032] The process flow of this embodiment is as figure 1 As shown, the structure of the sedimentation / magnetic separator used is as follows figure 2 As shown, the inner diameter of the sedimentation / magnetic separator is 0.6 meters, and two sets of electromagnets are used to achieve magnetic separation. Sintered metal filter tube, the filter element has a pore size of 5 microns, and the backwash interval is 30 minutes. The catalyst used is a cobalt-based Fischer-Tropsch synthesis catalyst supported on alumina, with a cobalt content of 20% (mass), an average particle size of 50 microns, and a catalyst concentration of 32% (mass) in the catalyst slurry drawn from the reactor. The operation process is as follows: (1) The slurry enters the sedimentation / magnetic separator, flows upward in area A and undergoes gravity sedimentation. When the slurry passes through area B, the electromagnet is energized for 180 seconds, the catalyst is sucked under the electromagnet, and the liqui...
Embodiment 5-7
[0036] The process flow of this embodiment is as figure 1 As shown, the structure of the sedimentation / magnetic separator used is as follows figure 2 As shown, the inner diameter of the sedimentation / magnetic separator is 0.6 meters, and two sets of electromagnets are used to achieve magnetic separation. Sintered metal filter tube, the filter element has a pore size of 5 microns, and the backwash interval is 30 minutes. The catalyst used is a Raney iron catalyst with an iron content of 75% (mass) and an average particle size of 45 microns. The catalyst concentration in the catalyst slurry drawn from the reactor is 32% (mass). The operation process is as follows: (1) The slurry enters the sedimentation / magnetic separator, flows upward in area A and undergoes gravity sedimentation. When the slurry passes through area B, the electromagnet is energized for 120 seconds, the catalyst is sucked under the electromagnet, and the liquid flows out of the sedimentation / magnetic separato...
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