Unlock instant, AI-driven research and patent intelligence for your innovation.

Liquid solid magnetic separation method

A technology of magnetic separation and magnetic separator, which is applied in the field of magnetic separation of Fischer-Tropsch synthesis heavy products and solid catalysts in a slurry bed, can solve the problems that fine particle catalysts are not easy to settle and carry out a lot of catalysts, and achieve continuous long-term cycle. Operational, easy to implement, efficient separation effect

Active Publication Date: 2014-06-11
CHINA PETROLEUM & CHEM CORP +1
View PDF5 Cites 12 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

When the sedimentation method is used alone for separation, because the fine particle catalyst is not easy to settle, the catalyst is carried over too much

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Liquid solid magnetic separation method
  • Liquid solid magnetic separation method
  • Liquid solid magnetic separation method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1-4

[0032] The process flow of this embodiment is as figure 1 As shown, the structure of the sedimentation / magnetic separator used is as follows figure 2 As shown, the inner diameter of the sedimentation / magnetic separator is 0.6 meters, and two sets of electromagnets are used to achieve magnetic separation. Sintered metal filter tube, the filter element has a pore size of 5 microns, and the backwash interval is 30 minutes. The catalyst used is a cobalt-based Fischer-Tropsch synthesis catalyst supported on alumina, with a cobalt content of 20% (mass), an average particle size of 50 microns, and a catalyst concentration of 32% (mass) in the catalyst slurry drawn from the reactor. The operation process is as follows: (1) The slurry enters the sedimentation / magnetic separator, flows upward in area A and undergoes gravity sedimentation. When the slurry passes through area B, the electromagnet is energized for 180 seconds, the catalyst is sucked under the electromagnet, and the liqui...

Embodiment 5-7

[0036] The process flow of this embodiment is as figure 1 As shown, the structure of the sedimentation / magnetic separator used is as follows figure 2 As shown, the inner diameter of the sedimentation / magnetic separator is 0.6 meters, and two sets of electromagnets are used to achieve magnetic separation. Sintered metal filter tube, the filter element has a pore size of 5 microns, and the backwash interval is 30 minutes. The catalyst used is a Raney iron catalyst with an iron content of 75% (mass) and an average particle size of 45 microns. The catalyst concentration in the catalyst slurry drawn from the reactor is 32% (mass). The operation process is as follows: (1) The slurry enters the sedimentation / magnetic separator, flows upward in area A and undergoes gravity sedimentation. When the slurry passes through area B, the electromagnet is energized for 120 seconds, the catalyst is sucked under the electromagnet, and the liquid flows out of the sedimentation / magnetic separato...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
Surface magnetic inductionaaaaaaaaaa
Surface magnetic inductionaaaaaaaaaa
Granularityaaaaaaaaaa
Login to View More

Abstract

A liquid solid magnetic separation method is characterized in that: in a settling magnetic separator, catalyst particles and a fischer-tropsch synthesis heavy product are preliminarily separated by gravity settling; separated slurry enters into a magnetic field zone, the catalyst particles are adsorbed by magnetic force in the magnetic field zone, the fischer-tropsch synthesis heavy product separated from the catalyst particles flows out from an outlet pipe, when the amount of the adsorbed catalyst particles reaches a certain amount, the magnetic field is removed, the catalyst particles sinks by gravity to a flow guide pipe, flows to the bottom of a settling tank, and is cycled to a reactor.

Description

technical field [0001] The invention relates to a solid-liquid separation method, in particular to a magnetic separation method of a slurry bed Fischer-Tropsch synthesis heavy product and a solid catalyst. Background technique [0002] With the changes in the world's energy structure and the increasing global environmental protection requirements, the method of preparing synthetic oil through Fischer-Tropsch synthesis using natural gas and coal-based syngas as raw materials has the advantages of clean products, no sulfur, nitrogen, and aromatic hydrocarbons, etc. In recent years, it has attracted the attention of countries all over the world. [0003] The core of Fischer-Tropsch synthesis technology is catalyst and reactor technology. Currently, Fischer-Tropsch synthesis catalysts mainly include cobalt catalysts and iron catalysts. In terms of reactors, the slurry bed Fischer-Tropsch synthesis reactor has the characteristics of convenient heat extraction, simple structure,...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): B03C1/32
Inventor 孟祥堃张晓昕王宣慕旭宏宗保宁聂红
Owner CHINA PETROLEUM & CHEM CORP