A kind of preparation method of wear-resistant and flame-retardant swash plate
A technology of swash plate and wear-resistant coating, which is applied in the field of preparation of swash plate of automobile air-conditioning compressors, can solve the problems of increasing preparation difficulty, harmful social environment, increasing social energy consumption, etc., and achieves simple and controllable preparation process and reasonable composition , The effect that the spraying thickness is easy to control
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Synthetic example 1
[0033] Synthesis Example 1 Synthesis of Silicon-containing Phosphate
[0034] Add 15mL bromotrimethylsilane, 5ml diethanolamine, 30ml absolute ethanol and 2g potassium silanolate to the three-necked flask, reflux and stir for 5 hours, cool, and filter to obtain the liquid; add 2.5ml, 50ml of 85% phosphoric acid to the liquid Acetone and 1.2g of phosphorus pentoxide were heated to 60°C, stirred and reacted for 2 hours, the acetone was removed by distillation, and the obtained liquid was silicon-containing phosphate.
Synthetic example 2
[0035] Synthesis Example 2 Preparation of Composite Filler
[0036] Mix 380g of molybdenum disulfide and 100g of aluminum phosphate evenly, sinter at 500°C for 55min, and crush it into a powder with a particle size of 15-22μm, which is the composite filler.
Embodiment 1
[0038] A wear-resistant and flame-retardant swash plate, the preparation of which comprises the following steps:
[0039] (1) Preparation of component A: in a nitrogen atmosphere, mix bisphenol A epoxy resin, maleic anhydride and ethylene glycol, react at 110°C for 35 minutes, then add 5 drops of sulfuric acid with a concentration of 30%, and continue the reaction for 7 minutes Obtain an epoxy compound; then react the epoxy compound with bisphenol A cyanate at 150°C for 15 minutes to obtain component A; wherein bisphenol A epoxy resin, maleic anhydride, ethylene glycol and bisphenol A cyanide The mass ratio of acid ester is 0.4: 1: 1.5: 1.5;
[0040](2) preparation of wear-resistant coating: dissolving component A in acetone to obtain mass concentration is the acetone solution of component A of 30%; then silicon-containing phosphate, PTFE particles, fluorinated graphite and composite filler are mixed uniformly, A solid lubricant is obtained; finally, the acetone solution of c...
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