225results about How to "Component distribution is even" patented technology

The invention relates to a process for manufacturing the molybdenum based rare earth alloy plate and equipment for manufacturing the same, wherein pure molybdenum powder is simultaneously added with four rare earth oxides of ZrO2, Y2O3, La2O3 and Nd2O3 according to certain ratio, by utilizing the chrematistics of long and large crystal grain and strong sag resistance and anti-creep property of rare earth alloy elements and the dispersion strengthening function, the re-crystallization temperature of the metal molybdenum is increased, the mechanical performances of the molybdenum based material such as tensile property, yielding behavior and extensibility are improved, and the application range of the molybdenum based material is widened; and the manufacturing process comprises production procedures of material preparation treatment, mixing treatment, forming treatment, sintering treatment, material making treatment and the like and the setting of various technical parameters of special technical equipment and process. With the preparation process, the molybdenum based rare earth alloy plate which has the advantages of good electric conductivity and heat conductivity, excellent high-temperature resistance and corrosion resistance and better mechanical performances such as tensile property, yielding behavior and extensibility, and fills in domestic blank and can replace the imported material can be manufactured.

The invention discloses a catalyst for synthesising methanol by hydrogenation of carbon dioxide. The catalyst is composed of oxides with the following molar ratio based on metal: 20-50% of La, 0-10% of M, 15-35% of Cu, and 2-15% of Zn, wherein M is one or more of Zr, Y, K, Ag, Ce, Pd, Mn, Mg, Fe, Co, Ni or Cr. The catalyst disclosed by the invention has the advantages that preparation is simple, operation is easy, catalyst performance repeatability is good, industrial amplification is easy to realize, and reaction conversion rate and reaction selectivity are high.

The present invention relates to a catalyst for making low-carbon mixed alcohol co-produced gasoline fraction from synthesis gas. The catalyst is characterized in that in weight percentage, the catalyst consists of 20 percent to 40 percent of Cu, 15 percent to 40 percent of Fe, 5 percent to 25 percent of Mn, 5 percent to 25 percent of Zn, 5 percent to 15 percent of Zr, 5 percent to 10 percent of Co and 0.01 percent to 5 percent of M, wherein, M is one kind or multiple kinds of alkali metals, alkaline earth metals or transition metal elements. The catalyst is prepared by a coprecipitation method. The catalyst has the advantages of low cost, good stability, long life and high selectivity of the low-carbon mixed alcohol co-produced gasoline fraction made from the synthesis gas under mild reaction condition.

The invention provides a preparation method of an oxygen-containing washing agent. The preparation method comprises the following steps of: A, adding 1-10 parts by weight of surfactant, 10-70 parts by weight of sodium carbonate, 1-40 parts by weight of sodium sulfate and a raw material combination containing or not containing additional assistant into a reactor, wherein the additional assistant contains 0-20 parts by weight of sodium bicarbonate, 0-30 parts by weight of silicious sodium salt and 0-10 parts by weight of an anti-dirt redeposition agent; and B, adding an aqueous hydrogen peroxide solution in the reactor, controlling the reaction temperature of the reactor to be 0-60 DEG C, shaping and drying after reaction to obtain 100 parts by weight of the oxygen-containing washing agent the active oxygen content of which is 1-12.33%. The invention also provides the oxygen-containing washing agent prepared by using the preparation method. The preparation method provided by the invention is safe and environment-friendly, and can prepare the oxygen-containing washing agent which has the advantages of uniform component distribution, variable active oxygen content, stable performance,and excellent washing effect.

The present invention relates to an iron-copper base catalyst synthesizing mixture of lower alcohols. In weight percentage, the iron-copper base catalyst consists of 20 percent to 60 percent of Cu, 15 percent to 60 percent of Fe, 0.4 percent to 20 percent of Mn, 0.4 percent to 30 percent of Zn and 0 percent to 5 percent of MA. The catalyst is prepared by a coprecipitation method. The iron-copper base catalyst has the advantages of simple preparation, easy operation, good reaction performance repeatability of the catalyst, realizing industrial amplification easily, good stability and high total alcohol selectivity.

The invention discloses a methanation catalyst for a fluidized bed and a preparation method of the methanation catalyst for the fluidized bed. The methanation catalyst for the fluidized bed comprises a carrier, an active component and auxiliary agents, and the active component and the auxiliary agents are loaded on the carrier. The carrier is a compound of Al2O3, ZrO2 and NiO or a compound of Al2O3, TiO2 and NiO; the active component is NiO; the auxiliary agents are oxides of at least one of Mg, Ca, La, Ce, Mn, Fe, Cu, Cr and Co. A co-precipitation method is adopted for preparation of the carrier of the catalyst, and uniformity in component distribution is realized; then spray forming is adopted to obtain the micro-spherical catalyst carrier which is high in fluidity and suitable for the fluidized bed. In preparation of the carrier of the catalyst, silicon sol or silicon-aluminum composite sol is added to serve as an adhesive; in a process of quick preparation of the micro-spherical carrier by spray forming, the silicon sol or silicon-aluminum composite sol is dispersed among carrier components, and after high-temperature calcination, the catalyst carrier is high in mechanical strength, abrasion resistance and impact resistance.

The invention belongs to the technical field of chemical preparations and in particular relates to a catching agent of benzene series compounds and a preparation method thereof. The catching agent of the benzene series compounds comprises the following raw materials in parts by weight: 5-8 parts of polyacrylamide, 10-20 parts of starch, 8-15 parts of sorbic acid, 10-15 parts of sodium sorbate, 30-45 parts of plant flower extractive, 5-10 parts of penetrating agent, 15-20 parts of sepiolite powder, 1-3 parts of cerium manganese compound oxide catalyst, 5-10 parts of cross-linked rectorite, 10-20 parts of chitosan and 80-100 parts of deionized water. The catching agent of the benzene series compounds is good in absorption and long in service life, so that the pollution caused by the benzene series compounds after decoration of a house is solved; meanwhile, the catching agent of the benzene series compounds is also capable of effectively inhibiting or killing some bacteria and viruses in influenza, intestinal tract and skin; the catching agent of the benzene series compounds is beneficial to the health of people.

The invention discloses a method for preparing a component from a laser additional material and a system for preparing the laser additional material, and relates to the technical field of preparing ofthe additional material. The problems that when the additional material is prepared through coaxial feeding and laser precipitating of premixed powder, due to the different ratio and the long-term and long-distance conveying, the airborne conveying segregation phenomenon and heavy-light separation phenomenon occur before the powder reaches a molten bath, and compositions in the composite component formed through laser precipitating are not evenly distributed are solved. A device for preparing the additional material through lasers is applied to the method. The method includes the steps that apowder feeder controls different types of material powder output by at least two powder feeding tanks to converge at a same position of a base material face according to the additional material preparing strategy of the component so that the different types of material powder output by at least two powder feeding tanks can flow on the base material face to form a mixture; and a laser device controls a laser machining head to perform melting and sintering on the mixture according to the additional material preparing strategy of the component to obtain the component. The method for preparing the component from the laser additional material and the system for preparing the laser additional material are used for preparing the additional material.

The invention relates to the technical field of nanomaterials, and in particular, relates to a method for preparing a metal oxide multistage structure by an MOF-derived bimetallic oxide template; theMOF-derived bimetallic oxide template is treated by an alkali to obtain the metal oxide multistage structure; M is set as a metal in the metal oxide multistage structure, the MOF-derived bimetallic oxide template is MMoO4-MOF-derived bimetallic oxide, and the metal oxide multistage structure is MxOy. The preparation process is simple, mild and universal, has no special requirements for equipment,does not use surfactants, and can be industrialized and produced in large scale. The metal oxide multi-stage structure prepared by the method is uniform in size, stable in structure and uniform in component distribution.

The invention relates to a high-catalytic activity composite negative electrode material of an intermediate-temperature solid oxide fuel cell and a preparation method of the composite negative electrode material, and belongs to the technical field of an energy material. The composite negative electrode comprises a perovskite structured oxide PrBa<1-x>Co<2>O<6-Delta>, Pr<1-y>BaCo<2>O<6-Delta> or Pr<1-n>Ba<1-m>Co<2>O<6-Delta> in the absence of A-position cation and an oxygen ion conductor material Sm<0.2>Ce<0.8>O<1.9> or Gd<0.1>Ce<0.9>O<1.95>, wherein the mass percent of the oxygen ion conductor material accounts for 20-50%. The preparation method of the composite negative electrode material comprises the following steps of firstly, respectively preparing synthesis solutions of two constituents; secondly, mixing and uniformly stirring the two solutions to obtain a mixed synthesis solution of the two constituents, and heating the mixed synthesis solution to obtain mixed precursor gel; and finally, carrying out high-temperature sintering reaction to obtain composite negative electrode powder. The composite negative electrode material is prepared by a synchronous sintering reaction method, the preparation method has the advantages of simplicity in process, short preparation period, low cost and high efficiency, and is easy to operate, and the oxygen reduction catalytic activity of the negative electrode of the intermediate-temperature solid oxide fuel cell is effectively improved.

The medical composite beta-tricalcium phosphate/collagen material consists of nano level beta-tricalcium phosphate in 50-67 wt% and collagen 33-50 wt%. Through in-situ complexing of collagen and beta-tricalcium phosphate, nanometer level beta-tricalcium phosphate powder is deposited on collagen substrate, and under the action of glutaraldehyde, the composite material has raised mechanical strength. The composite beta-tricalcium phosphate/collagen material of the present invention has homogeneous components, close combination, excellent biocompatibility, proper pore size and other features, and is suitable for use as the medical bone repairing material.

The invention discloses a preparation method of a metal selenide porous frame/graphene composite fiber. The metal selenide porous frame/graphene composite fiber is prepared from a fibrous compound asa precursor by calcining, and the fibrous compound is prepared from MOF (metal-organic framework) crystal powder and graphene oxide by compounding. The preparation method is simple to operate and mildin condition, the composite fiber is adjustable in morphology, controllable in structure and uniform in component distribution, structural integrity of graphene and a metal selenide porous frame obtained by taking MOF crystals as the template is retained, excellent performance of graphene and excellent performance of the metal selenide porous frame are combined, and the composite fiber can be produced in batches or industrially, has excellent performance as a lithium ion battery anode material and has good application prospect.

The invention discloses a toughened and reinforced nylon 6 ternary composite material and a preparation method thereof, belongs to the field of polymer composite materials and relates to a nylon 6 ternary composite material applied to automotive trim and some parts. The toughened and reinforced nylon 6 ternary composite material comprises the following components in parts by weight: 70-80 parts of nylon 6, 20-30 parts of thermoplastic elastomer and 0.5-1.5 parts of carbon nano tube. The prepared nylon 6 ternary composite material has excellent gap impact property and thermal property, the defect of nylon 6 that gap impact property is low can be overcome; meanwhile, bending property and tensile property of the nylon 6 still can be maintained; application field of the nylon 6 is further expanded; meanwhile, experimental raw materials are simple and easily available, and the preparation method is practicable.

A flexible graphene-based conductive composite thin film is disclosed. The composite thin film is composed of cellulose fibers, graphene and silver nanoparticles; the surface layer structure is a continuous silver nanoparticle film formed by mutually stacking silver nanoparticles, and the interior is composed of cellulose, graphene and silver nanoparticles. The cellulose fibers are skeletons, andthe inner silver nanoparticles are wrapped by graphene. The cellulose fiber-graphene-silver nanoparticle composite thin film of the structure has excellent conductivity with the square resistance being only 0.17 [omega]sq<-1>, and has excellent electrochemical performance; the maximum area specific capacitance is up to 1242.7 mF cm<-2>, and the rate performance is good; there is almost no loss ofcapacitance (the capacitance retention rate can still reach 99.7%) after 6000 times of repeated charge and discharge under the high current density of 60 mA cm<-2>, showing excellent the stability ofrepeated charge and discharge; and the energy density is high and the specific capacitance area is large.

The invention discloses a preparation method for a composite electrolyte membrane of a solid-state battery. By a multi-layer slope flowing coating process, multi-layer organic-inorganic composite electrolyte paste is synchronously coated on a surface of a carrier, and the composite electrolyte membrane of the multi-layer structure solid-state battery can be prepared. The multi-current coating process comprises the following steps of preparing paste of different constituents, allowing the organic-inorganic composite electrolyte paste to downwards flow along a slope flowing current after flowingout of a gap of a coating module according to an arrangement sequence, forming a liquid bridge in a gap between a coating roller and a slope flowing coating module, taking away by the running carrier, forming one or more layers of coating, performing, and stripping the carrier, thereby obtaining the composite electrolyte membrane of the solid-state battery.

The invention relates to tungsten-doped alloy powder and a preparing method thereof and belongs to the field of tungsten-based alloy materials. The preparing method of the tungsten-doped alloy powder comprises the following steps: 1, preparing a suspension A and a suspension B, wherein the suspension A is prepared by carrying out hydrothermal reaction on ammonium paratungstate under the condition that the pH is 1-1.2 and carrying out washing and sedimentation, and the suspension B is prepared by separately adding ammonium hydroxide into a zirconium nitrate solution and a yttrium nitrate solution and carrying out mixing, hydrothermal reaction, washing and sedimentation; 2, uniformly mixing the suspension A and the suspension B which are obtained in the step 1, and then, filtering and drying sediments so as to obtain precursor powder; and 3, forging the precursor powder obtained in the step 2 and carrying out reduction at a hydrogen atmosphere so as to obtain the tungsten-doped alloy powder. The tungsten-doped alloy powder which is obtained by adopting the preparing method has the advantages that the granularity of all components is small, the sizes of particles are more uniform, and the distribution of the components is more uniform.

The invention discloses a preparation method of metal sulfide porous framework/graphene composite fiber. The metal sulfide porous framework/graphene composite fiber is obtained through calcination with a fiber-like compound prepared by compounding MOF crystal powder and graphene oxide as a precursor. The preparation method is simple to operate, conditions are mild, the shape is adjustable, the structure is controllable, component distribution is uniform, the structural integrity of a metal sulfide porous framework obtained with graphene and MOF crystals as templates is kept, excellent properties of graphene and properties of the metal sulfide porous framework are integrated, the fiber can be produced in batches or industrially produced, and the fiber serves as a lithium ion battery negative electrode material, is excellent in performance and has a good application prospect.

The invention discloses a spiral low-shear static mixer, relates to a static mixer and in particular relates to a spiral low-shear static mixer. The invention aims to solve the problem that the conventional static mixer is high in viscosity loss and non-ideal in uniform mixing effect. The spiral low-shear static mixer comprises a tube shell and seven spiral mixing units, wherein the seven spiral mixing units are inserted into the tube shell; and the central line of each spiral mixing unit along the length direction is parallel to the central line of the tube shell along the length direction. The spiral low-shear static mixer is used for mixing polymer mother solution and water.

The invention relates to a method for preparing special-shaped lanthanum cuprate (La2CuO4) powder bodies by a sol-gel method. The method comprises the steps of: dissolving lanthanum nitrate and copper nitrate by de-ionized water to obtain a solution A; sequentially adding glycine and dispersants into the solution A, and adjusting the pH to be 1.5 to 4.5 with urea to obtain a solution B; standing, aging and drying the solution B to obtain dry gel; and grinding the dry gel into powders by a mortar, placing into a muffle furnace for calcining and grinding into powder to obtain the special-shaped La2CuO4 powder bodies. According to the method, the special-shaped La2CuO4 powder bodies are prepared by using the sol-gel method; EDTA (Ethylene Diamine Tetraacetic Acid), stearic acid and oxalic acid are used as dispersants respectively, so that the needle-like, rod-like and spindle-like La2CuO4 powder bodies can be obtained; the prepared La2CuO4 has the advantages of good crystallization, complete shape, good repeatability and low reaction temperature, so that the energy consumption is greatly reduced, the cost is saved; and the method is simple to operate and is suitable for large scale production.