Producing method of electrolytic copper powder

A technology for electrolytic copper powder and production method, which is applied to the improvement of process efficiency, photography process, instruments, etc., can solve problems such as affecting the quality of copper powder and consuming large natural gas energy, so as to improve quality, reduce energy consumption, and reduce production costs. Effect

Inactive Publication Date: 2014-06-18
CHONGQING YOUYAN ZHONGYE NEW MATERIAL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] The above traditional methods have the following disadvantages: the electrolytic copper plate is melted and cast into a cathode plate of a certain specification and shape, which will consume a large amount of natura

Method used

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  • Producing method of electrolytic copper powder
  • Producing method of electrolytic copper powder
  • Producing method of electrolytic copper powder

Examples

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Effect test

Embodiment 1

[0022] A kind of production method of electrolytic copper powder, it carries out as follows:

[0023] First, insert the raw material electrolytic copper plate into the conductive copper strip as the copper cathode plate, such as image 3 Shown—→Electrolysis in the electrolytic tank—→Electrolytic copper powder and mixed solution containing electrolyte—→Filtration and elutriation in the elutriation tank—→Filtration of wet electrolytic copper powder in the elutriation tank—→Water-containing electrolytic copper powder ——→Drying and reduction——→Dry electrolytic copper powder——→Crush and sieve powder——→Weighing and packaging——→Product.

[0024] The above electrolysis process uses 12 cathode plates and 13 anode plates in parallel, the concentration of copper ions in the electrolyte is 6g / L, the concentration of sulfuric acid is 133g / L, the electrolysis temperature is 45-48°C, the current in the electrolytic cell is 13000A, and the powder is scraped The time is 35 minutes / time, and ...

Embodiment 2

[0027] A kind of production method of electrolytic copper powder, it carries out as follows:

[0028] First, insert the raw material electrolytic copper plate into the conductive copper strip as the copper cathode plate, such as image 3 Shown—→Electrolysis in the electrolytic tank—→Electrolytic copper powder and mixed solution containing electrolyte—→Filtration and elutriation in the elutriation tank—→Filtration of wet electrolytic copper powder in the elutriation tank—→Water-containing electrolytic copper powder ——→Drying and reduction——→Dry electrolytic copper powder——→Crush and sieve powder——→Weighing and packaging——→Product.

[0029] The above electrolysis process uses 12 cathode plates and 13 anode plates connected in parallel, the copper ion concentration in the electrolyte is 5g / L, the sulfuric acid concentration is 150g / L, the electrolysis temperature is 50°C, the current in the electrolytic cell is 13000A, and the powder scraping time is 30 minutes / time, the electr...

Embodiment 3

[0032] A kind of production method of electrolytic copper powder, it carries out as follows:

[0033] First, insert the raw material electrolytic copper plate into the conductive copper strip as the copper cathode plate, such as image 3 Shown—→Electrolysis in the electrolytic tank—→Electrolytic copper powder and mixed solution containing electrolyte—→Filtration and elutriation in the elutriation tank—→Filtration of wet electrolytic copper powder in the elutriation tank—→Water-containing electrolytic copper powder ——→Drying and reduction——→Dry electrolytic copper powder——→Crush and sieve powder——→Weighing and packaging——→Product.

[0034] The above electrolysis process uses 12 cathode plates and 13 anode plates connected in parallel, the copper ion concentration in the electrolyte is 7g / L, the sulfuric acid concentration is 120g / L, the electrolysis temperature is 55°C, the current in the electrolytic cell is 13000A, and the powder scraping time is 40 minutes / time, the electr...

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Abstract

The invention discloses a producing method of electrolytic copper powder. The method comprises steps of: inserting an electrolytic copper plate that is a raw material into a conductive copper bar so as to adopt the inserted copper plate as a copper negative plate, electrolyzing in an electrolytic tank, filtering obtained electrolytic copper powder and a mixed solution containing electrolyte, elutriating, drying and reducing the wet electrolytic copper powder, smashing and screening. In the electrolytic process, the copper ion concentration in the electrolyte is 5-7 g/L, the sulfuric acid concentration is 120-150 g/L, the electrolytic temperature is 45-55 DEG C, the current in the electrolytic tank is 13000 A, the powder scrapping time is 30-40 min for one time of powder scrapping, and the electrolyte is fed in a manner of feeding in a direction parallel to the negative plate and the positive plate. The method omits a step of casting melt electrolytic copper into the positive plate of a certain specification and shapes, effectively reduces the production cost and improves the quality of the produced electrolytic powder. The produced electrolytic powder has a size not more than 200 meshes and is high in purity. Electrolysis can be normally performed in the electrolytic tank when the voltage is 1.6-1.8 volts, thus largely reducing the energy consumption. The electrolytic efficiency can be 80-85%.

Description

technical field [0001] The invention relates to a production method of electrolytic copper powder, in particular to a production method of electrolytic copper powder with low production cost. Background technique [0002] At present, the basic method of producing electrolytic copper powder is to produce the raw material electrolytic copper plate of copper powder (such as figure 1 [0003] shown) is melted in a copper furnace and cast into a small cathode plate of a certain specification (such as figure 2 shown), then put in the [0004] electrolysis in an electrolytic cell. Generally, there are the following procedures: [0005] Electrolytic copper plate——→Smelting in copper melting furnace——→Copper cathode plate——→Electrolysis in electrolytic tank——→ [0006] Electrolytic copper powder and mixed solution containing electrolyte ——→ Filtration and elutriation in the elutriation tank——→ Wet electrolytic copper powder [0007] ——→Drying and reduction——→Dry electroly...

Claims

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Application Information

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IPC IPC(8): C25C5/02C25C1/12
CPCY02P10/20
Inventor 向敏孟庆芳曾明军
Owner CHONGQING YOUYAN ZHONGYE NEW MATERIAL
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