Ternary solvent system aluminum nitride slurry formula for preparing high-heat conduction ceramic substrate
A high thermal conductivity ceramic and ternary solvent technology, applied in the field of aluminum nitride slurry formulation, can solve the problems of large dielectric constant, large difference in linear expansion coefficient, low thermal conductivity, etc., and achieve high bending strength and good suspension performance. , the effect of high thermal conductivity
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Embodiment 1
[0020] The ternary solvent system aluminum nitride slurry for preparing high thermal conductivity ceramic substrates includes 105 parts by weight of aluminum nitride powder, Y 2 o 3 3 parts by weight, 12 parts by weight of ethanol, 12 parts by weight of n-propanol, 24 parts by weight of butanol, 2 parts by weight of glycerin, 10 parts by weight of polyvinyl butyral, and 5 parts by weight of dibutyl phthalate.
[0021] 105 parts by weight of aluminum nitride powder, 3 parts by weight of Y 2 o 3 , 12 parts by weight of ethanol, 12 parts by weight of n-propanol, a mixture of 24 parts by weight of butanol, 2 parts by weight of oil glycerin and ball milling for 26 hours, then add 10 parts by weight of polyvinyl butyral, 5 parts by weight of o-phthalic The dibutyl diformate was mixed together for 12 hours, and then subjected to vacuum defoaming treatment for 5 hours to obtain a slurry with a viscosity of 22000 cps.
Embodiment 2
[0023] CaO, Al 2 o 3 , Y 2 o 3 、Dy 2 o 3 , B 2 o 3 , CaF 2 , Li 2 CO 3 , BN, Li 2 O. LiYO 2 , YF 3 and (CaY)F 5
[0024] The ternary solvent system aluminum nitride slurry for preparing high thermal conductivity ceramic substrates comprises 108 parts by weight of aluminum nitride powder, Li 2 CO 3 1 part by weight, CaF 2 3 parts by weight, Dy 2 o 3 2 parts by weight, 12.2 parts by weight of ethanol, 12.2 parts by weight of n-propanol, 24.4 parts by weight of butanol, 2.2 parts by weight of glycerin, 11 parts by weight of polyvinyl butyral, and 6 parts by weight of dibutyl phthalate. According to the method of Example 1, a slurry having a viscosity of 21500 cps was obtained.
Embodiment 3
[0026] The ternary solvent system aluminum nitride slurry for preparing high thermal conductivity ceramic substrates comprises 110 parts by weight of aluminum nitride powder, 1 part by weight of CaF, 1 part by weight of Al 2 o 3 5 parts by weight, Y 2 o 3 4 parts by weight, 12 parts by weight of ethanol, 12 parts by weight of isopropanol, 24 parts by weight of butanol, 2 parts by weight of glycerin, 10 parts by weight of polyvinyl butyral, and 6.7 parts by weight of dibutyl phthalate. According to the method of Example 1, a slurry having a viscosity of 21800 cps was obtained.
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