A method for detection of active ingredients in Qishen Yiqi dripping pills

A technology of Qishen Yiqi dropping pills and a detection method, which is applied in the directions of measuring device, material separation, material analysis, etc., can solve the problems of high price, cumbersome operation steps, poor accuracy, etc.
CN103926366BActive Publication Date: 2016-08-31TIANJIN TASLY PHARMA CO LTD
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Patents(China)
Current Assignee / Owner
TIANJIN TASLY PHARMA CO LTD
Publication Date
2016-08-31

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Abstract

The invention provides a detection method for effective components of an astragalus Salvia Miltiorrhiza qi-benefiting dropping pill. The method includes identification of panax notoginseng, astragalus and Dalbergia odorifera and tanshinol content determination. Specifically, the method consists of: preparing a panax notoginseng and astragalus test solution, preparing a panax notoginseng and astragalus reference solution, conducting panax notoginseng and astragalus thin-layer identification, preparing a Dalbergia odorifera test solution, preparing a Dalbergia odorifera reference drug solution, performing Dalbergia odorifera thin-layer identification, and determining the tanshinol content by ultra-high performance liquid chromatography. Tests show that the method has very good linearity, repeatability, reproducibility and stability, as well as high recovery rate, and is conducive to more comprehensive control of the quality of the astragalus Salvia Miltiorrhiza qi-benefiting dropping pill.
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Description

Technical field:

[0001] The invention belongs to the field of detection of traditional Chinese medicines, and in particular relates to an identification method and a content determination method of Qishen Yiqi dripping pills. Background technique:

[0002] Qishen Yiqi Dropping Pills (QSYQ) is a traditional Chinese medicine compound preparation composed of astragalus, salvia miltiorrhiza, notoginseng and balsamic oil. It was approved by the State Food and Drug Administration of China in 2003 for the treatment of coronary heart disease and angina pectoris. Stimulation, no obvious side effects.

[0003] Preclinical pharmacodynamic tests showed that Qishen Yiqi Dropping Pills can reduce the infarction size of dogs with myocardial infarction, improve ischemic electrocardiogram, reduce serum enzyme CK and LDH activity, reduce plasma ET and TXB2 levels, and reduce 6-Keto-PGF1α Activity and 6-Keto-PGF1α / TXB2 ratio increase; it can reduce the infarct size and increase SOD activity ...

Claims

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