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Silver-plating solution

A solution and silver-plating technology, applied in the field of metal surface treatment, can solve the problems of poor coating adhesion and no coating in deep concave parts, and achieve the effect of solving poor adhesion.

Inactive Publication Date: 2014-08-13
XIAN XIGUANG SURFACE FINISHING
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The purpose of the present invention is to solve the above technical problems and provide a silver plating solution to overcome the disadvantages of the existing silver plating technology, such as poor bonding force of the coating and no coating in the deep concave part.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] 1. Prepare 100L silver plating solution: 38g / L silver chloride AgCl, 95g / L analytically pure potassium cyanide KCN, 1.3g / L analytically pure sodium thiosulfate Na 2 S 2 o 3 .5H 2 O content is prepared.

[0021] Among them, silver chloride is prepared by adding sodium chloride to silver nitrate. Dissolve 5.7 kg of silver nitrate and 2 kg of sodium chloride in a separate container with an appropriate amount of water, and then dissolve the sodium chloride The solution is slowly poured into the silver nitrate solution while stirring continuously. At this time, a white curd-like silver chloride precipitate is precipitated. After standing still, the upper solution is poured out by decantation, and the chlorine remaining at the bottom is Wash silver with distilled water 2 to 3 times to remove Na + , NO 3 - and more Cl - Ion, standby, the whole operation process should be carried out in a dark room or place away from light.

[0022] Then 9.5 kg of potassium cyanide and ...

Embodiment 2

[0046] 1. Prepare 100L silver plating solution: 30g / L silver chloride AgCl, 70g / L analytically pure potassium cyanide KCN, 0.5g / L analytically pure sodium thiosulfate Na 2 S 2 o 3 .5H 2 O content is prepared.

[0047] Among them, silver chloride is prepared by adding sodium chloride to silver nitrate. Dissolve 5.7 kg of silver nitrate and 2 kg of sodium chloride in a separate container with an appropriate amount of water, and then dissolve the sodium chloride The solution is slowly poured into the silver nitrate solution while stirring continuously. At this time, a white curd-like silver chloride precipitate is precipitated. After standing still, the upper solution is poured out by decantation, and the chlorine remaining at the bottom is Wash silver with distilled water 2 to 3 times to remove Na + , NO 3 - and more Cl - Ion, standby, the whole operation process should be carried out in a dark room or place away from light.

[0048] Then 7 kg of potassium cyanide and 50...

Embodiment 3

[0072] 1. Prepare 100L silver plating solution: 45g / L silver chloride AgCl, 120g / L analytically pure potassium cyanide KCN, 2g / L analytically pure sodium thiosulfate Na 2 S 2 o 3 .5H 2 O content is prepared.

[0073] Among them, silver chloride is prepared by adding sodium chloride to silver nitrate. Dissolve 5.7 kg of silver nitrate and 2 kg of sodium chloride in a separate container with an appropriate amount of water, and then dissolve the sodium chloride The solution is slowly poured into the silver nitrate solution while stirring continuously. At this time, a white curd-like silver chloride precipitate is precipitated. After standing still, the upper solution is poured out by decantation, and the chlorine remaining at the bottom is Wash silver with distilled water 2 to 3 times to remove Na + , NO 3 - and more Cl - Ion, standby, the whole operation process should be carried out in a dark room or place away from light.

[0074] Then 12 kg of potassium cyanide and 20...

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PUM

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Abstract

The invention relates to a silver-plating solution, which belongs to the technical field of metal surface treatment. The silver-plating solution is composed of the following components: 30-45 g / L of newly-prepared silver chloride AgCl, 70-120 g / L of analytically pure potassium cyanide KCN, and 0.5-2 g / L of analytically pure sodium thiosulfate Na2S2O3.5H2O. Due to the adoption of the silver-plating solution disclosed by the invention, defects that the bonding force of plating layers is poor and deeply concave parts have no plating layer in existing silver-plating techniques can be overcome.

Description

technical field [0001] The invention relates to a design method of an electroplating process, in particular to a silver plating solution for metal materials such as aluminum, aluminum alloy, nickel and copper, and belongs to the technical field of metal surface treatment. Background technique [0002] Silver is a silver-white metal with an atomic weight of 108 and a density of 10.5. The electrochemical equivalent of silver is 4.025g / A.h, and the standard electrode potential of silver is 0.81V. The silver coating has good conductivity and solderability, and is easy to polish. High chemical stability. [0003] At present, the silver plating process is mainly used in electrical connectors, especially with the development of electronic technology in recent years, aluminum is widely used in the electronic field because of its cheap price, light weight, and easy processing. Therefore, aluminum Silver plating technology is particularly important, but the main problems existing in ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C25D3/46
Inventor 王新军李麦翠刘利于莉马健崔伟
Owner XIAN XIGUANG SURFACE FINISHING