Preparation and detecting methods of traditional Chinese medicine composition for treating wind-cold-wetness evil

A technology for wind-cold-dampness pathogens and compositions, which is applied in the field of preparation of traditional Chinese medicine compositions for treating wind-cold-dampness pathogens, which can solve the problems of backward detection methods, inconvenient taking, and difficult preparation of preparations, etc., and achieves a simple and easy preparation method with high accuracy , highly specific effect

Active Publication Date: 2014-09-17
CHANGCHUN RENMIN PHARMA GROUP
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0009] The invention provides a preparation method and a detection method of a traditional Chinese medicine composition for treati...

Method used

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  • Preparation and detecting methods of traditional Chinese medicine composition for treating wind-cold-wetness evil
  • Preparation and detecting methods of traditional Chinese medicine composition for treating wind-cold-wetness evil
  • Preparation and detecting methods of traditional Chinese medicine composition for treating wind-cold-wetness evil

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0056] The preparation method of embodiment 1 water honey pill

[0057] (a) 85.8g black snake with head and tail removed, 85.8g Nepeta, 85.8g Fangfeng, 68.2g vinegar Cyperus, 68.2g Duhuo, 68.2g ground beetle, 68.2g Clematis, 51.2g Guizhi, and 51.2g Qianghuo g, Dilong 51.2g, Zhichuanwu 34g, Zhicaowu 34g, crushed into coarse powder;

[0058] (b) Sterilization: spread the above coarse powder on a tray with holes all over the body, the thickness of the coarse powder is 5cm, set the temperature at 55°C, and keep warm for 2 hours;

[0059] (c) fine crushing: put the sterilized coarse powder of medicinal materials into a pulverizer and pulverize into fine powder, pass through a 100-mesh sieve, and batch mix for 45 minutes, and mix well;

[0060] (d) Refining honey: refining raw honey, removing froth, dead bees and impurities, making 50% refined honey for subsequent use;

[0061] (e) Pill making: use 80% medicinal powder and 50% refined honey to combine lumps, use 42g of 50% refined...

Embodiment 2

[0062] The preparation method of embodiment 2 water honey pill

[0063] (a) 85.8g black snake with head and tail removed, 85.8g Nepeta, 85.8g Fangfeng, 68.2g vinegar Cyperus, 68.2g Duhuo, 68.2g ground beetle, 68.2g Clematis, 51.2g Guizhi, and 51.2g Qianghuo g, Dilong 51.2g, Zhichuanwu 34g, Zhicaowu 34g, crushed into coarse powder;

[0064] (b) Sterilization: spread the above coarse powder on a tray with holes all over the body, the thickness of the coarse powder is 5cm, set the temperature at 50°C, and keep warm for 3 hours;

[0065] (c) fine crushing: put the sterilized coarse powder of medicinal materials into a pulverizer and pulverize into fine powder, pass through a 100-mesh sieve, and batch mix for 45 minutes, and mix well;

[0066] (d) Refining honey: refining raw honey, removing froth, dead bees and impurities, making 45% refined honey for subsequent use;

[0067] (e) Pill making: use 80% medicinal powder and 45% refined honey to combine lumps, use 40g of 45% refined...

Embodiment 3

[0068] The preparation method of embodiment 3 water honey pill

[0069] (a) 85.8g black snake with head and tail removed, 85.8g Nepeta, 85.8g Fangfeng, 68.2g vinegar Cyperus, 68.2g Duhuo, 68.2g ground beetle, 68.2g Clematis, 51.2g Guizhi, and 51.2g Qianghuo g, Dilong 51.2g, Zhichuanwu 34g, Zhicaowu 34g, crushed into coarse powder;

[0070](b) Sterilization: Take the above coarse powder and spread it in a tray with holes all over the body, the thickness of the coarse powder is 5cm, set the temperature at 60°C, and keep it warm for 1 hour;

[0071] (c) fine crushing: put the sterilized coarse powder of medicinal materials into a pulverizer and pulverize into fine powder, pass through a 100-mesh sieve, and batch mix for 45 minutes, and mix well;

[0072] (d) Refining honey: refining raw honey, removing froth, dead bees and impurities, making 55% refined honey for subsequent use;

[0073] (e) Pill making: use 80% medicinal powder and 55% refined honey to combine lumps, use 45g o...

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Abstract

The invention relates to preparation and detecting methods of a traditional Chinese medicine composition for treating wind-cold-wetness evil, belonging to the technical field of traditional Chinese medicines. The traditional Chinese medicine composition is prepared from zaocys dhumnades, schizonepeta, radix saposhnikoviae, prepared rhizoma cyperi with vinegar, radix angelicae pubescentis, ground beeltle, radix clematidis, cassia twig, notopterygium roots, earthworms, radix aconiti preparata and radix aconiti kusnezoffii preparata. The traditional Chinese medicine composition is prepared into easily swallowed pills by using a plastic molding and extensive preparation combined application technology, so that defects of the traditional Chinese medicine composition in clinical application are overcome. The detection for the composition is strengthened through the additional increment of thin-layer chromatography identification, meanwhile, the problem that spots on the limited amount of reference substances of aconitine as a toxic ingredient disappear instantly or do not appear is solved by using a thin layer chromatography, and a method for measuring 5-O-methylvisammioside as a main ingredient is improved by using a high-performance liquid chromatography, so that the technical problems that the content is not up to the standard under the condition that the quailed raw materials are put into production and the transfer rate of effective ingredients is relatively low are solved. The detecting method provided by the invention not only is suitable for industrial production, but also provides a safe and effective detecting means for clinical medication.

Description

technical field [0001] The invention belongs to the technical field of traditional Chinese medicines and natural medicines, and in particular relates to a preparation method and a detection method of a traditional Chinese medicine composition for treating wind-cold-damp pathogens. Background technique [0002] Rheumatic diseases are a class of autoimmune diseases that invade various tissues, systems and internal organs, which can cause damage to various tissues and organs, seriously affect their normal functions, and even cause fatal damage. At present, the most widely used in the market is "Shanhan Huoluo Pill", a traditional Chinese medicine composition with the main curative effect of chasing wind and cold, relaxing tendons and activating collaterals. , Difficulty walking, etc. It is used for shoulder and back pain, numbness of hands and feet, waist and leg pain, difficulty in walking, etc. caused by wind-cold-dampness. Its prescription consists of 85.8 parts by weight ...

Claims

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Application Information

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IPC IPC(8): A61K36/8905A61K9/20A61P29/00G01N30/90G01N30/02
Inventor 王士青隋义东崔延辉陈希曹晓平
Owner CHANGCHUN RENMIN PHARMA GROUP
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