Preparation method for multifunctional plastic additive
A plastic additive and multi-functional technology, which is applied in the chemical industry and can solve the problems of complex multi-functional additive methods, unenvironmental protection and user inconvenience.
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preparation example Construction
[0022] according to figure 1 As shown, a preparation method of a multifunctional plastic additive includes:
[0023] Step S1. Take 60 to 80 parts by weight of aliphatic acrylate urethane oligomer, 5 to 15 parts by weight of acrylate monomer, and 0 to 5 parts by weight of vinyl silicone oil and place it with a stirrer, condenser and In the three-necked flask of an isobaric funnel;
[0024] Step S2: Place the three-necked flask in a temperature-controlled oil bath;
[0025] Step S3: Weigh 0.5 to 2 parts by weight of the free radical initiator, mix it evenly, and place it in an equal pressure funnel;
[0026] Step S4: When the stirrer is in a stirring state, after the oil bath starts to heat to a set temperature, the isostatic funnel starts to drip the initiator solution;
[0027] Step S5: After reacting for a certain period of time, 0.1 to 0.2 parts by weight of antioxidant is added to obtain the auxiliary agent.
[0028] Wherein, the rotation speed of the stirrer during the reaction is ...
Embodiment 1
[0036] Take 60 g of aliphatic acrylate polyurethane oligomer, 10 g of methyl acrylate, and 2 g of vinyl triethoxy silane in a 100 ml three-necked flask with a stirrer, condenser and isobaric funnel. The three-necked flask is placed in the program In a temperature-controlled oil bath;
[0037] Then weigh 0.5 g of dicumyl peroxide initiator, mix it evenly, and place it in an equal pressure funnel;
[0038] When the stirrer is stirring at 200 rpm, the oil bath starts to heat to 165°C, and the isobaric funnel starts to drip the initiator solution at a rate of 30 drops / min;
[0039] After 4 hours of reaction, 168 0.2 g of antioxidant was added to obtain auxiliary agent 1.
Embodiment 2
[0041] Take 60g of aliphatic acrylate polyurethane oligomer, 10g of methyl acrylate, and 2g of vinyltrimethoxysilane in a 100ml three-necked flask with a stirrer, condenser and isobaric funnel. The three-necked flask is placed in a program control In a warm oil bath;
[0042] Then weigh 0.5 g of dicumyl peroxide initiator, mix it evenly, and place it in an equal pressure funnel;
[0043] When the stirrer is stirring at 200 rpm, the oil bath starts to heat to 165°C, and the isobaric funnel starts to drip the initiator solution at a rate of 30 drops / min;
[0044] After 4 hours of reaction, 168 0.2 g of antioxidant was added to obtain auxiliary agent 2.
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