Preparation method of sweet orange flavor for cigarettes

A technology of orange flavor and sweet orange, which is applied in the field of preparation of sweet orange flavor for cigarettes, can solve the problem of low utilization rate of sweet orange, achieve ideal application effect, improve utilization rate, and enhance practicability

Active Publication Date: 2014-11-05
HUBEI CHINA TOBACCO IND +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Among them, the Chinese patents "Preparation Method of Sweet Orange Essence Microcapsules" (Application No. 200810070712.5), "Preparation Method of Nano Sweet Orange Essence" (Application No. 200710047535.4) and "Preparation Method of Sweet Orange Essence Capsules" (Application No. 201010147903.4) Both use the existing sweet orange flavor or sweet orange extract to prepare follow-up products related to sweet orange flavor, and do not involve the preparation method of sweet orange tobacco flavor, and the utilization rate of sweet orange is not high

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0012] (1) Separate the peel and pulp of the sweet orange, and remove the light white pulp inside the peel. Wherein the sweet orange pulp is mashed and filtered to obtain fresh sweet orange juice. Soak the peeled peel in saturated calcium hydroxide aqueous solution for 12 hours, take it out, and wash it with tap water. The cleaned sweet orange peel is mechanically pressed to obtain sweet orange crude oil and sweet orange peel residue.

[0013] (2) crude oil refinement: add 2 times the weight of 75% ethanol solution to the sweet orange crude oil in step (1), stir well and let stand for 6h, then utilize high-speed tubular centrifuge (rotating speed 9000r / min) Centrifuge for 10 minutes, remove the terpenoid components in the upper part of the centrifuge tube and the flocculent particles in the lower part, and obtain the sweet orange essential oil ethanol solution.

[0014] (3) essential oil preparation: add its weight 12% propylene glycol solution to the sweet orange essential ...

Embodiment 2

[0020] (1) Separate the peel and pulp of the sweet orange, and remove the light white pulp inside the peel. Wherein the sweet orange pulp is mashed and filtered to obtain fresh sweet orange juice. Soak the peeled peel in saturated calcium hydroxide aqueous solution for 18 hours, take it out, and clean it with tap water. The cleaned sweet orange peel is mechanically pressed to obtain sweet orange crude oil and sweet orange peel residue.

[0021] (2) Crude oil refinement: Add 5 times the weight of 95% ethanol solution to the sweet orange crude oil in step (1), stir well and let stand for 12 hours, then use a high-speed tubular centrifuge (rotating speed 6000r / min) Centrifuge for 10 minutes, remove the terpenoid components in the upper part of the centrifuge tube and the flocculent particles in the lower part, and obtain the sweet orange essential oil ethanol solution.

[0022] (3) essential oil preparation: add its weight 3% propylene glycol solution to the sweet orange essent...

Embodiment 3

[0028] (1) Separate the peel and pulp of the sweet orange, and remove the light white pulp inside the peel. Wherein the sweet orange pulp is mashed and filtered to obtain fresh sweet orange juice. Soak the peeled peel in saturated calcium hydroxide aqueous solution for 12 hours, take it out, and clean it with tap water. The cleaned sweet orange peel is mechanically pressed to obtain sweet orange crude oil and sweet orange peel residue.

[0029] (2) Crude oil refining: add 3 times the weight of 60% ethanol solution to the sweet orange crude oil in step (1), stir well and let stand for 6 hours, then use a high-speed tubular centrifuge (rotating speed 8500r / min) Centrifuge for 10 minutes, remove the terpenoid components in the upper part of the centrifuge tube and the flocculent particles in the lower part, and obtain the sweet orange essential oil ethanol solution.

[0030] (3) essential oil preparation: add its weight 5% propylene glycol solution to the sweet orange essential...

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PUM

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Abstract

The invention provides a method for preparing a sweet orange flavor for cigarettes. The method comprises the following steps: separating sweet orange peels from sweet orange pulp, squeezing the sweet orange pulp, extracting the sweet orange peels, and squeezing the extracted sweet orange peels to obtain sweet organic crude oil and sweet orange pomace; extracting the sweet orange crude oil by using ethanol, centrifuging the extracted sweet orange crude oil to obtain a sweet orange essential oil ethanol solution, and adding a propylene glycol solution to obtain sweet orange essential oil; extracting the sweet orange pomace by using ultrasonic waves to obtain an extracting solution a, adding sodium dihydrogen phosphate honey, sweet orange juice and apple vinegar into the extracting solution a in sequence, uniformly mixing the materials, and fermenting the mixture; extracting a fermentation product, and concentrating the extracted fermentation product to obtain a sweet orange pomace extract; and mixing the sweet orange essential oil and the sweet orange pomace extract, filtering a mixed extracting solution, adding D-sorbitol linalool oxide into a filtrate, and uniformly stirring the filtrate to obtain the sweet orange flavor for the cigarettes. By adopting the method, the utilization ratio of sweet oranges is increased; moreover, the preparation method is simple; and the prepared sweet orange flavor for the cigarettes is strong and real in fragrance, has an ideal application effect in the cigarettes, and has very high practicability.

Description

technical field [0001] The invention relates to a method for preparing tobacco spices, in particular to a method for preparing sweet orange spices for tobacco. Background technique [0002] Sweet orange is a kind of common fruit, which is widely distributed in all parts of our country. Because it is rich in vitamin C, organic acid, sugar and other ingredients, it has high nutritional value and is deeply loved by people. At present, sweet orange and related extracts are mainly used to prepare raw materials for food and cosmetic products, and less used to prepare tobacco flavors. Among them, the Chinese patents "Preparation Method of Sweet Orange Essence Microcapsules" (Application No. 200810070712.5), "Preparation Method of Nano Sweet Orange Essence" (Application No. 200710047535.4) and "Preparation Method of Sweet Orange Essence Capsules" (Application No. 201010147903.4) They all use the existing sweet orange flavor or sweet orange extract to prepare follow-up products rela...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/02A24B15/24
Inventor 喻世涛熊国玺苗立坤陈金强
Owner HUBEI CHINA TOBACCO IND
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