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Cationic chemical plugging agent and preparation method thereof

A plugging agent and cationic technology, which is applied in the field of cationic chemical plugging agent and its preparation, can solve the problems of low plugging success rate, poor plugging effect, little change in viscosity, etc., so as to achieve easy operation of plugging construction, improve Pressure-bearing capacity, the effect of a simple composition

Active Publication Date: 2014-11-19
CHINA PETROLEUM & CHEM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These constructions also have the following problems: first, the cost of urea-formaldehyde resin is high; second, the construction is difficult; third, when the drilling fluid is polluted or the ambient temperature changes, the urea-formaldehyde plugging agent is not easy to consolidate, resulting in a low plugging success rate
[0006] The existing chemical plugging agents have a certain plugging effect in field application, but they often show limitations such as low plugging efficiency, weak plugging strength, and short plugging validity period.
Analysis of the main reason for the low success rate of traditional plugging technology in drilling engineering is that the plugging agent and drilling fluid do not have a synergistic effect, the viscosity changes little after mixing, and the flow resistance of the plugging agent cannot be significantly improved. The plugging agent cannot form a certain volume of retention and solidification, resulting in poor plugging effect

Method used

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  • Cationic chemical plugging agent and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1~5

[0027] According to the formula shown in Table 1, configure 5 parts (respectively corresponding to Examples 1 to 5) of 1000g cationic chemical plugging agent, the specific operation steps are as follows: Take a 2500ml beaker and install a cantilever stirrer; Add water in an appropriate amount, start stirring, and the rotation speed is 450r / min; add cationic polyacrylamide (CP-9, produced by Shanghai Hengli Water Treatment Material Co., Ltd.) in the amount shown in Table 1, and stir for 2 hours to make the cationic polyacrylamide Dissolve; then add bentonite and calcium carbonate (average particle size: 0.06 μm) in sequence, and continue to stir to disperse evenly; then add hexamethylenetetramine, and continue to stir for 1 hour to obtain the viscous cations of Examples 1 to 5 Chemical plugging agent.

[0028] Table 1

[0029]

[0030] (2) Preparation of drilling fluid

[0031] 1000ml of conventional anionic polysulfide drilling fluid was prepared to measure the pressure-b...

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Abstract

The invention provides a cationic chemical plugging agent including 0.1-5 wt% of a cationic polymer, 1-15 wt% of a filler, 0.1-5 wt% of a crosslinking agent and 1-5 wt% of a rheological modifier, and the weight ratios are based on the total weight of the cationic chemical plugging agent. The cationic polymer is preferably a cationic polyacrylamide, the filler, the crosslinking agent and the rheological modifier are respectively preferably calcium carbonate, hexamethylenetetramine and bentonite. The cationic chemical plugging agent used in oil well leaking stoppage construction is mixed with an anionic drilling fluid in a well section with occurrence of well leakage, and then neutralization reaction and cross-linking reaction are performed, the mixed liquor viscosity increases rapidly, and a space network structure is formed, so that a leakage passage is blocked, the plugging effect is played, and the cationic chemical plugging agent ahs the characteristics of short time plugging consuming and high plugging efficiency.

Description

technical field [0001] The invention relates to the field of petroleum drilling, in particular to a cationic chemical plugging agent and a preparation method thereof. Background technique [0002] Drilling fluid loss (lost circulation) is a ubiquitous petroleum engineering technical problem that has not been completely resolved so far in the process of petroleum drilling. Especially in the drilling construction of deep wells and complex formations, formations with low pressure, fractures and karst caves are often encountered. According to incomplete statistics, the annual cost of dealing with well leakage in my country is as high as 200 million yuan. Therefore, developing a convenient and effective oilfield drilling plugging technology or providing an efficient and practical plugging agent will bring good economic and social benefits. [0003] During the drilling process, when drilling into high-permeability formations, especially formations with developed fractures or lar...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/42
CPCC09K8/426
Inventor 苏长明赵梦云苏建政张汝生马玉生郑承纲张锁兵
Owner CHINA PETROLEUM & CHEM CORP
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