Amoxicillin and potassium clavulanate capsule drug composition
A technology of amoxicillin sodium and clavulanate potassium and clavulanate potassium, which is applied in the field of amoxicillin sodium and clavulanate potassium capsule pharmaceutical composition, and can solve the problems of high content, unfavorable clinical use stability and drug efficacy stability and other problems, to achieve the effect of uniform particle size distribution, simple and comprehensive matching, and reduce the amount of related substances
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Embodiment 1
[0024] Amoxicillin sodium clavulanate potassium capsule pharmaceutical composition comprises following components by weight:
[0025] Amoxicillin 12.0
[0026] Potassium clavulanate 3.0
[0027] Microcrystalline cellulose 11.5
[0028] Magnesium stearate 0.2.
[0029] The specific rotation of amoxicillin is +290°.
Embodiment 2
[0031] Amoxicillin sodium clavulanate potassium capsule pharmaceutical composition comprises following components by weight:
[0032] Amoxicillin 12.48
[0033] Potassium clavulanate 3.12
[0034] Microcrystalline Cellulose 12.0
[0035] Magnesium stearate 0.4.
[0036] The specific rotation of amoxicillin is +306°.
Embodiment 3
[0038] Amoxicillin sodium clavulanate potassium capsule pharmaceutical composition comprises following components by weight:
[0039] Amoxicillin 14.6
[0040] Potassium clavulanate 3.65
[0041] Microcrystalline Cellulose 12.0
[0042] Magnesium stearate 0.6.
[0043] The specific rotation of amoxicillin is +295°.
[0044] Above embodiment all can adopt following preparation method, comprise the following steps:
[0045] (1) Preparation of potassium clavulanate: Slowly add the crude potassium clavulanate dropwise into the lower alcohol that has been dissolved in a small amount of potassium clavulanate crystals in advance, and keep stirring. When precipitation occurs, let it stand for 1-2 hours Then add the same amount of clavulanic acid potassium crystals as before, continue to stir for 5-10min, and then let it stand for 0.5-1h, control the entire ambient temperature during this process to 10-18°C, and then vacuum vacuum and dry to obtain clavulanic acid The pure potassi...
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Abstract
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