Production method for preparing monocalcium phosphate byproduct used as special fertilizer for chives
A technology of calcium dihydrogen phosphate and calcium hydrogen phosphate, which is applied in the direction of ammonium orthophosphate fertilizer, alkaline orthophosphate fertilizer, phosphate fertilizer, etc., can solve problems such as difficulty in meeting application requirements, environmental pollution, pollution, etc., and achieve long-term utilization of soil High efficiency, avoiding a lot of waste, and reducing production costs
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0048] A production method for preparing calcium dihydrogen phosphate by-product leek special fertilizer, comprising the following steps:
[0049] (1) Preparation and mixing of raw materials: Phosphoric acid and carbonamide are placed in a stirred reactor at a molar ratio of 1.1:1, at a temperature of 80°C, and the stirring speed of the stirred tank is controlled at 180r / min to stir and mix for 2 hours to obtain an intermediate slurry;
[0050] (2) Preparation of calcium hydrogen phosphate: Add soluble calcium salt into the reaction kettle containing the intermediate slurry prepared in step 1) at a constant speed for 2 hours, control the pH value to 3, continue stirring and reacting for 10 minutes, and the reaction ends to obtain Slurry containing calcium hydrogen phosphate;
[0051] (3) Cyclic crystallization and filtration: place the slurry containing calcium hydrogen phosphate obtained in step 2) in a cooling crystallizer to cool down to a temperature of 20°C within 15s, c...
Embodiment 2
[0058] A production method for preparing calcium dihydrogen phosphate by-product leek special fertilizer, comprising the following steps:
[0059] (1) Preparation and mixing of raw materials: Phosphoric acid and carbonamide are placed in a stirred reactor at a molar ratio of 2.0:1, at a temperature of 100°C, and the stirring speed of the stirred tank is controlled at 200r / min to stir and mix for 3 hours to obtain an intermediate slurry;
[0060] (2) Preparation of calcium hydrogen phosphate: Add soluble calcium salt 3h at a constant speed to the reaction kettle containing the intermediate slurry obtained in step 1), control the pH value to 3.5, continue stirring and reacting for 15min, and the reaction ends to obtain Slurry containing calcium hydrogen phosphate;
[0061] (3) Cyclic crystallization filtration: place the slurry containing calcium hydrogen phosphate obtained in step 2) in a cooling crystallizer to cool down to a temperature of 15°C within 15 seconds, cool down t...
Embodiment 3
[0069] A production method for preparing calcium dihydrogen phosphate by-product leek special fertilizer, comprising the following steps:
[0070] (1) Preparation and mixing of raw materials: Put phosphoric acid and carbonamide at a molar ratio of 1.5:1 in a stirred reactor at a temperature of 90°C and control the stirring speed of the stirred tank at 190r / min to stir and mix for 2.5 hours to obtain intermediate body slurry;
[0071] (2) Preparation of calcium hydrogen phosphate: Add soluble calcium salt into the reaction kettle containing the intermediate slurry obtained in step 1) at a constant speed for 2.5 h, control the pH value to 3.3, continue stirring and reacting for 13 minutes, and the reaction ends. Obtain the slurry containing calcium hydrogen phosphate;
[0072] (3) Cyclic crystallization filtration: place the slurry containing calcium hydrogen phosphate obtained in step 2) in a cooling crystallizer to cool down to a temperature of 18°C within 15s, cool down to...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com