A kind of manganese-carbon catalytic inner electrolytic filler and its preparation method and application
A technology of internal electrolysis and manganese carbon, which is applied in the direction of chemical instruments and methods, water treatment parameter control, multi-stage water treatment, etc., can solve the problems of difficulty in increasing the removal rate, packing compaction, and affecting the treatment effect, so as to improve the chemical reaction rate , high COD removal rate, rapid and thorough response
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Embodiment 1
[0040] Mix 75g of manganese ore waste and 75g of activated carbon, grind them, and pass through a 100-130 mesh sieve. Then add kaolin 40g, coal powder 15g, mix and stir evenly. Slowly shake it after adding a certain amount of water to form spherical particles with a particle size of 1-2 mm. Then put it into a muffle furnace and gradually raise the temperature to 70-80°C at a rate of 3-5°C / min, continue drying for 20 minutes, steam the water out, and finally sinter the above-mentioned manganese-carbon material at 1100°C under the condition of nitrogen filling for 2 hours, and roast After the completion, the packing is taken out and cooled to obtain the manganese-carbon catalytic inner electrolytic packing with a specific surface area of 1.30m 2 / g, the porosity is 66%. 200ml solution with COD concentration of 3000mg / L, adjust the pH to 3, put 200g of manganese carbon electrolytic material into it, after aeration for 2 hours, adjust the pH to 8, remove the supernatant to mea...
Embodiment 2
[0042]Mix 75g of manganese ore waste and 75g of activated carbon, grind them, and pass through a 100-130 mesh sieve. Then add kaolin 40g, coal powder 15g, mix and stir evenly. Slowly shake it after adding a certain amount of water to form spherical particles with a particle size of 3-5 mm. Then put it into a muffle furnace and gradually raise the temperature to 70-80°C at a rate of 3-5°C / min, continue drying for 20 minutes, steam the water out, and finally sinter the above-mentioned manganese-carbon material at 1100°C under the condition of nitrogen filling for 2 hours, and roast After the completion, the packing is taken out and cooled to obtain the manganese-carbon catalytic inner electrolytic packing with a specific surface area of 1.13m 2 / g, the porosity is 65%. 200ml solution with COD concentration of 3000mg / L, adjust the pH to 3, put 200g of manganese carbon electrolytic material into it, after aeration for 2 hours, adjust the pH to 8, remove the supernatant to meas...
Embodiment 3
[0044] Mix 75g of manganese ore waste and 60g of activated carbon, grind them, and pass through a 100-130 mesh sieve. Then add kaolin 40g, coal powder 15g, mix and stir evenly. Slowly shake it after adding a certain amount of water to form spherical particles with a particle size of 1-2 mm. Then put it into a muffle furnace and gradually raise the temperature to 70-80°C at a rate of 3-5°C / min, continue drying for 20 minutes, steam the water out, and finally sinter the above-mentioned manganese-carbon material at 1100°C under the condition of nitrogen filling for 2 hours, and roast After the completion, the packing is taken out and cooled to obtain the manganese-carbon catalytic inner electrolytic packing with a specific surface area of 1.28m 2 / g, the porosity is 65%. 200ml solution with COD concentration of 3000mg / L, adjust the pH to 3, put 200g of manganese carbon electrolytic material into it, after aeration for 2 hours, adjust the pH to 8, remove the supernatant to mea...
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