Method for simultaneously determining multiple preservatives in exported vegetables
A method of determination and technology of preservatives, applied in the field of chemical analysis and detection, can solve the problems of vegetable preservation quality decline, economic loss, easy spoilage and mildew, etc., and achieve short time consumption, high accuracy and precision, and simple detection steps Effect
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[0053] The specific implementation of the present invention will be further described below in conjunction with the examples. The following examples are used to illustrate the present invention, but are not intended to limit the scope of the present invention.
[0054] 1) extract
[0055] Use a homogenizer to make vegetable homogenate from the original vegetables, weigh 10.00g vegetable homogenate (accurate to 0.01g) into a 50mL offline tube, add 20mL n-hexane-ethyl acetate (1+2, V / V) solution , vortex and mix for 2 minutes, shake horizontally for 5 minutes, then add 5.00g (accurate to 0.01g) sodium chloride, vortex and mix again for 1min, 5000r / min offline for 3min, draw 10mL supernatant Ⅰ into a 15mL offline tube, To be purified.
[0056] 2) Purify the sample
[0057] Weigh 100mg of ethylenediamine-N-propylsilane (PSA, 60μm) and 500mg of anhydrous sodium sulfate into 10mL of supernatant Ⅰ, vortex and mix for 2min, 5000r / min off-line for 3min, draw supernatant Ⅱ into 25mL...
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