A method for determining the content of seven components in a traditional Chinese medicine composition preparation
A determination method and composition technology, which can be used in measurement devices, material separation, and analysis of materials, etc., can solve the problems of long inspection period, many components, and not ideal, and achieve fast analysis speed, good repeatability, and convenient control. Effect
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Embodiment 1
[0056] The raw material drug formula is:
[0057] Polygonum multiflorum 200g Suanzaoren 200g Mulberry 200g Ganoderma lucidum 100g Lily 100g
[0058] Anemarrhena 66.7g Salvia miltiorrhiza 166.7g Chrysanthemum 66.7g Poria cocos 100g Albizia julibrissin 200g
[0059] The preparation method of Chinese medicine composition tablet is:
[0060] a) Proportionally weigh the cleaned Polygonum multiflorum, Anemarrhena, and selected crude jujube kernels, add 60% ethanol, heat and reflux to extract twice, add 10 times the amount for the first time, extract for 2 hours, and add 8 times for the second time. Double the amount, extract for 1 hour, filter the extracts, combine them, recover ethanol under reduced pressure, concentrate until the relative density measured at 60°C is 1.10, and obtain the alcohol extraction extract, which is set aside;
[0061] b) Weigh the selected mulberry fruit, poria cocos, ganoderma lucidum, salvia miltiorrhiza, albizia julibrissin, and chrysanthemum in propo...
Embodiment 2
[0072] The raw material drug formula is:
[0073] Polygonum multiflorum 150g Suanzaoren 275g Mulberry 160g Ganoderma lucidum 80g Lily 160g
[0074] Anemarrhena 110 grams, Salvia miltiorrhiza 120 grams, chrysanthemum 120 grams, Poria cocos 75 grams, Albizia Julibrissin 288 grams.
[0075] The preparation method of Chinese medicine composition capsule is:
[0076] a) Weigh the cleaned Polygonum Polygoni Multiflori, Zhimu and the selected coarse jujube kernels in proportion, add 6 times the amount of 30% ethanol, heat and reflux to extract 3 times, each time for 3 hours, filter the extract, combine, and recover under reduced pressure Ethanol, concentrated until the relative density measured at 60°C is 1.15, to obtain the alcohol extraction extract, set aside;
[0077] b) Weigh the selected mulberry fruit, poria cocos, ganoderma lucidum, salvia miltiorrhiza, albizia julibrissin, and chrysanthemum in proportion, add 10 times the amount of water to extract 3 times, extract for 3 h...
Embodiment 3
[0094] The raw material drug formula is:
[0095] Polygonum multiflorum 270g Suanzaoren 145g Mulberry 255g Ganoderma lucidum 135g Lily 75g
[0096] Anemarrhena 50 grams, Salvia miltiorrhiza 120 grams, chrysanthemum 45 grams, Poria cocos 145 grams, Albizia Julibrissin 165 grams.
[0097] The preparation method of Chinese medicine composition pill is:
[0098] a) Weigh the cleaned Polygonum multiflorum multiflorum, Anemarrhena anemarrhenae, and selected coarse jujube kernels in proportion, add 12 times the amount of 70% ethanol, heat and reflux to extract twice, each time for 2 hours, filter the extract, combine, and recover under reduced pressure Ethanol, concentrated until the relative density measured at 60°C is 1.12, to obtain the alcohol extraction extract, for subsequent use;
[0099] b) Weigh the selected mulberry fruit, poria cocos, ganoderma lucidum, salvia miltiorrhiza, albizia julibrissin, and chrysanthemum in proportion, add 15 times the amount of water to extract ...
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