Preparation method of novel nano-material used for biosensor
A biosensor and nanomaterial technology, applied in the field of preparation of new nanomaterials, can solve the problems of high surface energy, easy to be oxidized, poor dispersion, etc., achieve good paramagnetism and magnetic responsiveness, and the preparation method is simple and easy, high The effect of antioxidant capacity
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[0019] figure 1 It is a process step diagram of a novel nanomaterial preparation method for a biosensor in an embodiment of the present invention; the novel nanomaterial is a walnut-structured maghemite / silicon dioxide composite magnetic nanoparticle, and the preparation method includes the following steps: a) preparation of maghemite nanoparticles, b) hydrolysis and condensation treatment of maghemite nanoparticles, c) washing and drying treatment.
[0020] The preparation method of the novel nanomaterial used for biosensors mentioned in the present invention is by adding the maghemite nanoparticles with a particle diameter of about 40nm into the tetraethyl orthosilicate gel system, hydrolyzing and condensing, and using The maghemite / silica composite magnetic nanoparticles with core-shell structure were prepared by sol-gel method. The silica in the composite magnetic nanoparticles has excellent chemical stability and high temperature resistance. At the same time, the unsatur...
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[0022] The specific preparation method is as follows:
[0023] a) Preparation of maghemite nanoparticles, the specific preparation process is as follows: first put ferric chloride powder and sodium hydroxide powder into a grinder at a mass ratio of 7:4, and then add polyethylene glycol-200 to continue grinding for 30 minutes , wherein, the dosage ratio of polyethylene glycol-200 and ferric chloride powder is 1.25ml / g; then the product after grinding is repeatedly washed three times with deionized water and absolute ethanol, and put into Dry in a vacuum oven at 70°C for 2 hours to obtain a precursor product; finally, roast the precursor product at 500°C for 1 hour to obtain maghemite nanoparticles.
[0024] b) Hydrolysis and condensation treatment of maghemite nanoparticles. The specific preparation process is as follows: first, add a certain amount of prepared maghemite nanoparticles into a container containing absolute ethanol and water, and ultrasonically disperse them for 3...
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