Medical antibacterial material and preparation method thereof

A technology of antibacterial materials and antioxidants, applied in the field of medical antibacterial materials and their preparation, can solve problems such as unsatisfactory antibacterial performance, and achieve the effect of good comprehensive performance and wide application.

Inactive Publication Date: 2015-02-25
中新态(厦门)环保科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] With the improvement of the quality of human life, the research on medical antibacterial materials has developed rapidly, but the antibacterial performance of the medical antibacterial materials currently used is not ideal, and the general antibacterial rate can reach 80-90%. With the conti

Method used

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  • Medical antibacterial material and preparation method thereof
  • Medical antibacterial material and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0024] A medical antibacterial material, comprising by weight components: 65 parts of PE, 0.8 part of antioxidant CA, 0.8 part of co-antioxidant DLTP, 3 parts of butyl acetate, 1 part of sodium carbonate, 5 parts of tall oil fatty acid, 5 parts of lauryl betaine, 0.5 part of sodium tripolyphosphate, 0.8 part of sodium xylene sulfonate, 1 part of dodecyl dimethyl benzyl ammonium chloride.

[0025] The preparation method of above-mentioned medical antibacterial material, comprises the following steps:

[0026] Step 1: Add PE, butyl acetate and tall oil fatty acid to the reaction kettle, add sodium carbonate, lauryl betaine, sodium tripolyphosphate, sodium xylene sulfonate and dodecyl dimethyl benzyl chloride Dissolve ammonium chloride in 20 parts of water, then add it into the reaction kettle, stir and mix evenly under the condition of 50°C, the stirring speed of stirring and mixing evenly is 150 rpm, the mixing time is 20 minutes, and then under the vacuum degree of 0.02MPa Ra...

Embodiment 2

[0030] A medical antibacterial material, comprising by weight components: 70 parts of PE, 1 part of antioxidant CA, 1 part of co-antioxidant DLTP, 6 parts of butyl acetate, 2 parts of sodium carbonate, 7 parts of tall oil fatty acid, 6 parts of lauryl betaine, 0.6 part of sodium tripolyphosphate, 1.2 parts of sodium xylene sulfonate, 1 part of dodecyl dimethyl benzyl ammonium chloride.

[0031] The preparation method of above-mentioned medical antibacterial material, comprises the following steps:

[0032] Step 1: Add PE, butyl acetate and tall oil fatty acid to the reaction kettle, add sodium carbonate, lauryl betaine, sodium tripolyphosphate, sodium xylene sulfonate and dodecyl dimethyl benzyl chloride Dissolve ammonium chloride in 22 parts of water, then add it into the reaction kettle, stir and mix evenly at 53°C, the stirring speed of stirring and mixing is 160 rpm, the mixing time is 25 minutes, and then under the vacuum degree of 0.03MPa Raise the temperature to 82°C, ...

Embodiment 3

[0035] A medical antibacterial material, comprising by weight components: 75 parts of PE, 1.2 parts of antioxidant CA, 1.2 parts of co-antioxidant DLTP, 7 parts of butyl acetate, 3 parts of sodium carbonate, 8 parts of tall oil fatty acid, 7 parts of lauryl betaine, 0.7 parts of sodium tripolyphosphate, 1.4 parts of sodium xylene sulfonate, 2 parts of dodecyl dimethyl benzyl ammonium chloride.

[0036] The preparation method of above-mentioned medical antibacterial material, comprises the following steps:

[0037] Step 1: Add PE, butyl acetate and tall oil fatty acid to the reaction kettle, add sodium carbonate, lauryl betaine, sodium tripolyphosphate, sodium xylene sulfonate and dodecyl dimethyl benzyl chloride Dissolve ammonium chloride in 26 parts of water, then add it to the reaction kettle, stir and mix evenly at 55°C, wherein the stirring speed of stirring and mixing is 180 rpm, the mixing time is 30 minutes, and then under the vacuum degree of 0.04MPa Raise the tempera...

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Abstract

The invention discloses a medical antibacterial material and a preparation method thereof. The medical antibacterial material comprises the following components: PE, an antioxidant, an assistant antioxidant, butyl acetate, sodium carbonate, tall oil fatty acid, lauryl betaine, sodium tripolyphosphate, sodium xylene sulfonate, and dodecyl dimethyl benzyl ammonium chloride. The preparation method comprises the following steps of adding PE, butyl acetate and tall oil fatty acid into a reaction kettle, dissolving sodium carbonate, lauryl betaine, sodium tripolyphosphate, sodium xylene sulfonate, and dodecyl dimethyl benzyl ammonium chloride in water and then adding the solution into the reaction kettle, uniformly stirring and mixing at a certain temperature, reacting under stirring and heating conditions in vacuum, heating and reacting under stirring to obtain a first mixture; adding the antioxidant and the assistant antioxidant into the first mixture, uniformly stirring and mixing at a certain temperature and finally extruding in a twin-screw extruder. The medical antibacterial material provided by the invention has excellent antibacterial effect, is environmentally friendly and harmless and can be widely used.

Description

technical field [0001] The invention belongs to the technical field of medical material preparation, and in particular relates to a medical antibacterial material and a preparation method thereof. Background technique [0002] Pathogenic microorganisms such as bacteria and fungi often cause pathological changes in body tissues, seriously threatening human physical and mental health. According to the statistics of the World Health Organization (WHO) in 1998, there were 52 million deaths in the world in 1995, of which about 33% were caused by bacterial infections, and this ratio is still increasing today. Therefore, the development of medical antibacterial materials and products has received more and more attention. [0003] Medical antibacterial materials can effectively reduce the risk of the body getting sick by blocking, inhibiting or killing pathogenic microorganisms. A good medical antibacterial material should have the following characteristics: [0004] 1) The mater...

Claims

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Application Information

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IPC IPC(8): C08L23/06C08K13/02C08K3/26C08K5/09C08K5/19C08K3/32C08K5/42B29C47/92B29B7/00B29C48/92
CPCB29C48/92C08K3/26C08K3/32C08K5/09C08K5/19C08K5/42C08K13/02C08K2003/262C08K2003/324C08L23/06
Inventor 金仲恩全春兰张帆
Owner 中新态(厦门)环保科技有限公司
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