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Method for preparing hard alloy zinc molten material bar

A cemented carbide and zinc melting technology, which is applied to other manufacturing equipment/tools, mechanical equipment, turbines, etc., can solve the problems of cemented carbide quality degradation, hardness reduction, and low product density, and achieve low cost and easy control , excellent performance

Inactive Publication Date: 2015-03-04
XIAMEN YURUI CEMENTED CARBIDE TOOLS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

These will reduce the quality of cemented carbide products, especially the lower density and lower hardness of the product.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0019] As a specific embodiment, a method for preparing a cemented carbide zinc melt bar includes the following steps:

[0020] Mixture wet grinding processing: use zinc fusion carbide (WC) tungsten powder with an average particle size of less than 0.8um, cobalt (Co) powder with an average particle size of less than 2um, and carbon (C) powder with an average particle size of less than 400nm, among which cobalt (Co) powder It accounts for 10% of the total raw materials; carbon (C) powder accounts for 5.6% of the total raw materials. The above-mentioned raw materials use anhydrous alcohol (purity above 99.99%) as the medium, and the wet grinding process is used to match the quality of the alloy balls with the total raw materials. The ratio is 6:1; the ratio of anhydrous alcohol to the total raw materials is 300ml / kg; the wet grinding time is 60 hours; the wet-milled mixture is sieved with a 50-mesh vibrating screen,

[0021] Drying: add the mixture of the previous process to the diss...

Embodiment 2

[0026] As a specific embodiment, a method for preparing a cemented carbide zinc melt bar includes the following steps:

[0027] Mixture wet grinding processing: use zinc fusion carbide (WC) tungsten powder with an average particle size of less than 0.8um, cobalt (Co) powder with an average particle size of less than 2um, and carbon (C) powder with an average particle size of less than 400nm, among which cobalt (Co) powder It accounts for 15% of the total raw materials; carbon (C) powder accounts for 6.6% of the total raw materials. The above raw materials use anhydrous alcohol (purity above 99.99%) as the medium, and the wet grinding process is used to match the quality of the alloy balls with the total raw materials. The ratio is 6:1; the ratio of anhydrous alcohol to the total raw materials is 300ml / kg; the wet grinding time is 80 hours; the wet-milled mixture is sieved with a 50-mesh vibrating screen,

[0028] Drying: add the mixture of the previous process to the dissolved 52° ...

Embodiment 3

[0033] As a specific embodiment, a method for preparing a cemented carbide zinc melt bar includes the following steps:

[0034] Mixture wet grinding processing: use zinc fusion carbide (WC) tungsten powder with an average particle size of less than 0.8um, cobalt (Co) powder with an average particle size of less than 2um, and carbon (C) powder with an average particle size of less than 400nm, among which cobalt (Co) powder Accounting for 13% of the total raw materials; carbon (C) powder accounted for 5.6%-6.6% of the total raw materials, using anhydrous alcohol (above 99.99% purity) as the medium for the above raw materials, using wet grinding technology, alloy balls and total raw materials The mass ratio is 6:1; the ratio of anhydrous alcohol to the total raw materials is 300ml / kg; the wet milling time is 70 hours; the wet milled mixture is sieved with a 50-mesh vibrating screen,

[0035] Drying: add the mixture of the previous process to the dissolved 52° paraffin, add the paraffi...

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Abstract

The invention relates to the technical field of utilizing zinc molten material circulation for hard alloy preparation, in particular to a method for preparing a hard alloy zinc molten material bar. The method comprises the steps of selecting zinc molten wolfram carbide (WC) powder, cobalt (Co) powder and carbon (C) powder, wherein the mass of the Co powder occupies 10%-15% of total raw material mass, and the mass of the C powder occupies 5.6%-6.6% of the total raw material mass; carrying out wet grinding processing on a mixture, stirring and drying the mixture by adding the mixture which is obtained in the previous process in dissolved 52-EDG C paraffin, carrying out extrusion forming by adopting a hydraulic screw rod extrusion machine, carrying out vacuum drying on a formed bar by adopting a vacuum drying oven, and carrying out a sintering process. The method for preparing the hard alloy zinc molten material bar, disclosed by the invention, has the characteristics that the technological process is simple, the control is easy, the cost is low, the density of a produced product is high, the performance is excellent, and the like.

Description

Technical field [0001] The invention relates to the technical field of using zinc melt recycling for cemented carbide preparation, in particular to a method for preparing cemented carbide zinc melt rods. Background technique [0002] Since the raw materials used in the preparation of cemented carbide are very expensive, the ability to recycle cemented carbide waste has attracted much attention. After the waste cemented carbide is processed by the zinc melting method to obtain the zinc melt, it is recycled to the production of cemented carbide. Compared with the use of unused raw materials, the use of recycled cemented carbide will significantly reduce energy consumption and environmental impact. [0003] However, due to the Zn recovery process in the zinc melting method, the cemented carbide scrap is immersed in the molten zinc in the electric furnace. The zinc is then distilled at a certain temperature and thus removed from the furnace. The remaining powder contains WC separate...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F5/00B22F1/00B22F3/16
Inventor 罗跃谟陈胜书肖九生连长升林伟
Owner XIAMEN YURUI CEMENTED CARBIDE TOOLS