Method for simultaneously preparing potassium nitrate and calcium chloride from calcium nitrate solution and potassium chloride
A technology of potassium chloride and calcium nitrate, applied in the preparation of alkali metal nitrate, calcium/strontium/barium chloride, calcium/strontium/barium halide, etc., can solve the problems of low product yield and low purity of by-products, etc. Achieve the effect of high product purity, improved separation effect and high yield
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[0017] Example 1
[0018] Prepare 1640g of 30% calcium nitrate solution and add it to a stainless steel reactor with coil heating and jacket cooling. Then add 447g of potassium chloride solid to the calcium nitrate solution and heat it until all the potassium chloride solids are dissolved. The mixed solution is concentrated. When the surface of the mixed solution just appears crystallization, that is, when it reaches saturation, the heating is stopped. The temperature of the material is controlled by the jacket cooling water. When the temperature drops to 58°C, 223.5g of methanol (equivalent to 50% of the mass of potassium chloride), continue to lower the temperature and crystallize under stirring conditions, and continue stirring for 60 minutes to ensure that the potassium nitrate crystals are fully analyzed. When the temperature drops to 25°C, all the crystalline materials are precipitated, and the solids are separated by suction filtration. Wash the solid with potassium nitrat...
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[0020] Example 2
[0021] Prepare 1640g of 30% calcium nitrate solution and add it to a stainless steel reactor with coil heating and jacket cooling. Then add 447g of potassium chloride solid to the calcium nitrate solution and heat it until all the potassium chloride solids are dissolved. The mixed solution is concentrated. When the surface of the mixed solution just appears crystallization, that is, when it reaches saturation, the heating is stopped. The temperature of the material is controlled by the jacket cooling water. When the temperature drops to 50°C, 330g of methanol (equivalent to chlorine) is added to the reactor. 74% of the mass of potassium chloride), continue to lower the temperature and crystallize under stirring conditions, continue to stir for 180 minutes to ensure that the potassium nitrate crystals are fully analyzed, control the temperature through the refrigeration system and when the temperature drops to -20°C, all the crystalline materials are precipitated...
Example Embodiment
[0022] Example 3
[0023] Prepare 1640g of 30% calcium nitrate solution and add it to a stainless steel reactor with coil heating and jacket cooling. Then add 447g of potassium chloride solid to the calcium nitrate solution and heat it until all the potassium chloride solids are dissolved. The mixed solution is concentrated. When the surface of the mixed solution just appears crystallization, that is, when it reaches saturation, the heating is stopped. The temperature of the material is controlled by the jacket cooling water. When the temperature drops to 50°C, 223.5g of methanol (equivalent to 50% of the mass of potassium chloride), continue to lower the temperature and crystallize under stirring conditions, continue to stir for 30 minutes to ensure that the potassium nitrate crystals are fully analyzed, and control the temperature through the refrigeration system and when the temperature drops to -10°C, all the crystalline materials will be precipitated and the solid Separate b...
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