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Short-wavelength X-ray diffraction plate-like internal stress fixed-point non-destructive testing method

An internal stress, non-destructive testing technology, used in material analysis, measuring devices, instruments, etc. using wave/particle radiation, which can solve problems such as difficulty in guaranteeing, increasing test errors, and labor and time-consuming

Inactive Publication Date: 2015-04-08
SOUTHWEST TECH & ENG INST +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The usual X-ray diffraction method, using an ordinary X-ray tube, can only non-destructively measure the average stress of the material / workpiece surface with a thickness of about 10 microns, that is, the usual X-ray diffraction method can only non-destructively measure the surface stress
To non-destructively measure the internal stress of materials / workpieces, neutron diffraction of nuclear reactors or short-wavelength X-ray diffraction of high-energy synchrotron radiation is usually used. However, the cost and maintenance costs of these two devices are high, and in the world, using The method of nondestructively measuring the internal stress of materials / workpieces by using neutron diffraction to prepare stress-free standard sample technology is relatively mature, and the testing and research of using these two methods to nondestructively measure the internal stress of materials / workpieces in my country is still in progress
Among the disclosed test methods for short-wavelength X-ray instruments using heavy metal target X-ray tubes as the radiation source, the invention patent application number ZL201010586489.7 also discloses a fixed-point non-destructive testing method for the internal inspection of rolled aluminum alloy plates. The method of rolling residual stress and lateral residual stress, which adopts W target X-ray tube radiation, and obtains the reference original interplanar spacing d through the prepared stress-free standard sample 0 , measure the rolling direction and transverse strain, and calculate the rolling direction residual stress and transverse residual stress inside the rolled plate. This method needs to prepare a stress-free standard sample, which is not only labor-intensive and time-consuming, but also difficult to ensure the internal residual stress of the prepared stress-free standard sample. The value is zero, which increases the test error and affects the non-destructive testing of the internal residual stress of the material / workpiece

Method used

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  • Short-wavelength X-ray diffraction plate-like internal stress fixed-point non-destructive testing method

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Embodiment 1

[0038] The tested sample is a cuboid A100 steel block with a φ=14mm through hole in the middle. Its length is 120mm, its width is 40mm, and its thickness is 2.5mm. In order to improve the fatigue performance, the inner cylinder of the φ=14mm through hole of the sample The surface is processed by strong extrusion, and the prefabricated compressive stress field is used to suppress the fatigue crack growth, and its texture is weak. According to the following method steps, non-destructively detect the radial residual stress at the middle layer of the sample (1.25mm from the upper and lower surfaces respectively) and 4.6mm from the inner cylindrical surface of the through hole:

[0039] (1) Select the short-wavelength characteristic X-ray Kα of the heavy metal target X-ray tube used for measurement 1 : According to the short-wavelength characteristic X-ray WKα of the W-target X-ray tube 1 The energy is 59.3kev (corresponding to WKα 1 Wavelength λ=0.0208992nm), WKα 2 The energy i...

specific Embodiment 2

[0056] The tested sample is a friction stir welded part of 2024 aluminum alloy plate with a length of 300mm, a width of 200mm, and a thickness of 6mm. The weld length is 280mm, and the texture of the weld is weak. According to the following method steps, the middle layer of the sample (3 mm from the upper and lower surfaces respectively), the longitudinal residual stress in the center of the weld and its distribution along the length of the weld are tested non-destructively:

[0057] (1) Select the short-wavelength characteristic X-ray Kα of the heavy metal target X-ray tube used for measurement 1 : According to the short-wavelength characteristic X-ray WKα of the W-target X-ray tube 1 The energy is 59.3kev (corresponding to WKα 1 wavelength λ=0.0208992nm), set the upper threshold of the energy analyzer of its X-ray detection and analysis system to be 60.0kev and the lower threshold to be 58.6kev, and its X-ray detection and analysis system will only measure the short-wavelen...

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Abstract

Residual stress is generated inside a polycrystalline material after the polycrystalline material (such as aluminum alloy and steel) is machined. The invention provides a short-wavelength X-ray diffraction plate-like internal stress fixed-point non-destructive testing method aiming at a polycrystalline plate-like material or plate-like workpiece with a weak texture by utilizing a short-wavelength X-ray diffraction instrument. The method is used for directly measuring a certain (hkl) crystal face diffraction spectrum in a plurality of phi angle (wherein phi is more than or equal to 45 degrees and less than or equal to 90 degrees) directions, and calculating based on the Bragg principle and a stress-strain relationship of in the generalized Hooke's law to obtain the stress of a measured part in the measured direction. With the method, through the translation of X, Y and Z, the stress of the other part can be measured; the stress in the other direction can be measured by allowing the plate-like material or plate-like workpiece to rotate around the normal of a plate surface. For the polycrystalline plate-like material or plate-like workpiece with the weak texture, the stress of any part inside the polycrystalline plate-like material or plate-like workpiece in any direction of an XY plane can be measured.

Description

technical field [0001] The invention relates to a fixed-point non-destructive detection method for the internal stress of a plate-shaped sample that does not require a stress-free standard sample by using short-wavelength characteristic X-ray diffraction, and is suitable for the internal stress of plate-shaped materials and workpieces prepared from polycrystalline materials with weak textures. and nondestructive testing of its distribution. Background technique [0002] Polycrystalline materials (such as aluminum alloy, steel, etc.) often generate large residual stress inside the polycrystalline material due to uneven plastic deformation after pressure processing, heat treatment, welding, casting, etc. , resulting in deformation due to rebalancing of internal residual stress, and the degree of deformation is directly related to the internal residual stress and its distribution of the material before machining. Not only that, the mechanical properties of the material / workpie...

Claims

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Application Information

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IPC IPC(8): G01N23/207
Inventor 郑林张鹏程肖勇张津何长光彭正坤窦世涛
Owner SOUTHWEST TECH & ENG INST
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