Method for producing carbon-containing titanium sponge and device thereof
A technology of sponge titanium and carbon content, which is applied in the field of non-ferrous metal smelting, can solve the problems of addition and uneven addition, and achieve the effects of adding carbon elements, ensuring ingredients, and solving negative effects
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Embodiment 1
[0026] Feed amount based on five tons of reduction furnace: 20 tons of titanium tetrachloride (industrial grade), 32 kg of carbon tetrachloride (analytical pure). The preparation method of carbon-containing titanium sponge is as follows:
[0027] (1) Control the pressure in the titanium tetrachloride storage tank 7 at 0.03-0.06MPa, maintain the positive pressure state in the titanium tetrachloride storage tank, and supplement argon when it is lower than 0.03MPa to maintain the titanium tetrachloride storage tank. Tank pressure within the specified range of 0.03 ~ 0.06Mpa;
[0028] (2) Add the titanium tetrachloride of above-mentioned amount afterwards, and add the carbon tetrachloride of above-mentioned amount in stirring, carbon tetrachloride adds flow rate and is 800~1000ml / min, fully mixes with agitator 6, makes tetrachloride Carbon is fully dissolved in titanium tetrachloride;
[0029] (3) the mixed carbon tetrachloride and titanium tetrachloride mixture is added in the ...
Embodiment 2
[0032] Feed amount based on five tons of reduction furnace: 20 tons of titanium tetrachloride (industrial grade), 64 kg of carbon tetrachloride (analytical pure). The preparation method of carbon-containing titanium sponge is as follows:
[0033] (1) Control the pressure in the titanium tetrachloride storage tank 7 at 0.03-0.06MPa, maintain the positive pressure state in the titanium tetrachloride storage tank, and supplement argon when it is lower than 0.03MPa to maintain the titanium tetrachloride storage tank. Tank pressure within the specified range of 0.03 ~ 0.06Mpa;
[0034] (2) Add the titanium tetrachloride of above-mentioned amount afterwards, and add the carbon tetrachloride of above-mentioned amount in stirring, carbon tetrachloride adds flow rate and is 800~1000ml / min, fully mixes with agitator 6, makes tetrachloride Carbon is fully dissolved in titanium tetrachloride;
[0035] (3) the mixed carbon tetrachloride and titanium tetrachloride mixture is added in the ...
Embodiment 3
[0038]Feed amount based on five tons of reduction furnace: 20 tons of titanium tetrachloride (industrial grade), 128 kg of carbon tetrachloride (analytical pure). The preparation method of carbon-containing titanium sponge is as follows:
[0039] (1) Control the pressure in the titanium tetrachloride storage tank 7 at 0.03-0.06MPa, maintain the positive pressure state in the titanium tetrachloride storage tank, and supplement argon when it is lower than 0.03MPa to maintain the titanium tetrachloride storage tank. Tank pressure within the specified range of 0.03 ~ 0.06Mpa;
[0040] (2) Add the titanium tetrachloride of above-mentioned amount afterwards, and add the carbon tetrachloride of above-mentioned amount in stirring, carbon tetrachloride adds flow rate and is 800~1000ml / min, fully mixes with agitator 6, makes tetrachloride Carbon is fully dissolved in titanium tetrachloride;
[0041] (3) the mixed carbon tetrachloride and titanium tetrachloride mixture is added in the ...
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