Shale micropore size and fluid distribution analysis method
An analysis method and technology of microscopic pores, which are applied in the fields of suspension and porous material analysis, permeability/surface area analysis, and analysis by nuclear magnetic resonance, etc. Problems such as small ratio, to achieve rapid reproducibility, less damage to the core of the measurement, and the effect of protecting experimental resources
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[0032] The shale cores of the embodiment of the present invention are taken from the reef dam area, and the shale cores are processed with reference to the "SY / T6490-2007 Laboratory Measurement Specifications for NMR Parameters of Rock Samples", and the actual microscopic pore radius of the shale is obtained through the analysis of this example The distribution is compared with the shale pore radius size distribution tested by the liquid nitrogen-mercury porosimetry instrument. The two are very similar. This embodiment can reflect the advantages of the accuracy of the experimental method described in the present invention and the rapid and non-destructive measurement. The steps are as follows, such as Figure 6 Shown:
[0033] 1. Collect shale gas reservoir rocks and make natural cores. The diameter of the cores is about 2.5cm and the length is 2-5cm. Put the cores into a vacuum oven with a temperature of 120°C and a vacuum of -0.1MPa to dry for 8 Hours, remove a small amount...
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