A kind of slurry, reference gas layer and its preparation method and oxygen sensor
A gas layer and slurry technology, applied in the direction of instruments, scientific instruments, analytical materials, etc., can solve the problems of poor oxygen sensor performance, poor shape retention and tolerance of the reference channel, unsuitable for industrial operation, etc., to achieve shape retention and the effect of good tolerance, good performance, good shape retention and tolerance
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preparation example Construction
[0074] The invention provides a kind of preparation method of reference gas layer, comprising:
[0075] The slurry is printed on the surface of the reference channel and dried to obtain a reference air layer, and the slurry is the slurry described in the above technical solution.
[0076] In an embodiment of the present invention, the printing thickness may be 85 microns to 120 microns; in other embodiments, the printing thickness may be 90 microns to 110 microns. In an embodiment of the present invention, the printing speed may be 4cm / s~6cm / s; in other embodiments, the printing speed may be 4.5cm / s~5.5cm / s; in another In an embodiment, the printing speed may be 5 cm / s.
[0077] In an embodiment of the present invention, the distance between the screen and the substrate during the printing process may be 3 mm to 5 mm; in other embodiments, the distance between the screen and the substrate during the printing process may be 3.5 mm to 4.5 mm ; In another embodiment, the distan...
Embodiment 1
[0112] Add 40g of graphite powder with a particle size of 12500 mesh into a beaker, add 15g of turpentine and 25g of terpineol to the beaker, stir with a glass rod, and mix well to obtain a mixed solution;
[0113] The beaker was placed in warm water at 55°C, and 10 g of melamine resin was added to the mixed solution while stirring until the melamine resin was completely dissolved to obtain an intermediate mixture;
[0114] Take out the beaker, after the intermediate mixture is cooled to 25°C, add 3g of dispersant, 6g of plasticizer, 3g of leveling agent and 3g of wetting agent to the intermediate mixture, and transfer the resulting mixed product to Alumina ball milling beads were added to a ball mill jar made of zirconia, and ball milled at a speed of 320 rpm for 24 hours to obtain a slurry.
[0115] The viscosity of the slurry prepared in Example 1 of the present invention was tested using a DV-II rotational viscosity tester provided by BROOKFIELD, USA. The test result showe...
Embodiment 2
[0117] Add 55g of graphite powder with a particle size of 4000 mesh into the beaker, add 28g of isopropanol into the beaker, stir with a glass rod, and fully mix to obtain a mixed solution;
[0118] The beaker was placed in warm water at 50°C, and 12 g of acrylic resin was added to the mixture while stirring until the acrylic resin was completely dissolved to obtain an intermediate mixture;
[0119] Take out the beaker, after the intermediate mixture is cooled to 25°C, add 1g of dispersant, 2g of plasticizer, 1g of leveling agent and 1g of wetting agent to the intermediate mixture, and transfer the resulting mixed product to Alumina ball milling beads were added into a ball mill jar made of zirconia, and ball milled at a speed of 300 rpm for 20 hours to obtain a slurry.
[0120] The viscosity of the slurry prepared in Example 2 of the present invention was tested using a DV-II rotational viscosity tester provided by BROOKFIELD Corporation of the United States. The test result ...
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