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A method and device for measuring the complete evaporation temperature of alcohol-based fuel

A technology of complete evaporation temperature, alcohol-based fuel, applied in the investigation phase/state change and other directions, can solve the problems of inability to initialize the method, error in test results, etc., and achieve the effect of simple and convenient measurement method, proper control, and fast heat conduction

Active Publication Date: 2017-12-19
GUODIAN SCI & TECH RES INST +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In order to solve the above problems, the present invention provides a method for measuring the complete evaporation temperature of alcohol-based fuels, which can avoid the problem that the existing methods cannot be initialized, the measurement method is simple and convenient, and the error of the test results is small

Method used

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  • A method and device for measuring the complete evaporation temperature of alcohol-based fuel
  • A method and device for measuring the complete evaporation temperature of alcohol-based fuel
  • A method and device for measuring the complete evaporation temperature of alcohol-based fuel

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Embodiment 1

[0031] Embodiment 1: Alcohol-based fuel complete evaporation temperature measuring device

[0032] like figure 1 As shown, the measuring device includes a reactor 1 and an electric furnace 2, the electric furnace 2 is set on the outer wall of the reactor 1, the reactor 1 includes a kettle body 11 and a kettle cover 12, and two thermocouple sensors TC1 and TC2 are installed on the kettle cover 12 And a pressure sensor P, when the lid of the kettle is closed, TC1 is in contact with the bottom of the kettle body, and TC2 is suspended from the kettle body. The kettle body 11 and the kettle cover 12 are made of T316S ultra-low carbon stainless steel. The inner diameter of the kettle body 11 is 63.5mm and the volume is 500ml. TC2 is a K-type thermocouple sensor, and TC2 is 15mm away from the bottom of the kettle body.

Embodiment 2

[0033] Embodiment 2: take a certain alcohol-based fuel as an example to illustrate the principle of the measurement method of the present invention

[0034] Take the test results of a certain alcohol-based fuel as an example for analysis. Depend on figure 2 It can be seen that TC1 and TC2 have two "steps" with relatively gentle slopes during the heating process. Since the alcohol-based fuel is mainly made of methanol and ethanol mixed in different proportions, these two "steps" should be due to the It is produced when methanol and ethanol are evaporated separately. Unlike the horizontal boiling curve under constant pressure conditions, since the number of moles of the gas phase gradually increases during boiling in a constant volume reactor, the pressure in the vessel increases, and the corresponding saturation temperature also increases accordingly, resulting in a certain The slope of the boiling curve. However, it can be seen that the heating rate during boiling is signi...

Embodiment 3

[0038] Embodiment 3: Take water as the accuracy of the sample analysis method of the present invention

[0039] Measure different volumes of water (the volume corresponding to 1.45Mpa is 5.5ML, the volume corresponding to 1.99Mpa is 8ml, and the volume corresponding to 2.38Mpa is 9ml)) and add them to the constant-volume reactor described in Example 1; Install the lid of the reaction kettle to ensure the sealing fit between the kettle body and the lid; set the heating temperature of the heating device to 300°C through the temperature control unit, and start heating; after the temperature of the electric furnace reaches 300°C, first start the data processing unit, and then install the A good reaction kettle is placed in the heating device and heated at a constant temperature of 300°C. The liquid temperature and steam temperature in the kettle body are collected by thermocouple sensors TC1 and TC2 respectively. The data processing unit receives the temperature signal and draws th...

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Abstract

The invention discloses a method and a device for measuring the complete evaporation temperature of alcohol-based fuel. The method steps include: measuring alcohol-based fuel and adding it into the body of the constant-volume reactor; installing the lid of the constant-volume reactor; setting the heating temperature of the heating device of the reactor; and starting the data acquisition system after the temperature of the heating device of the reactor reaches the set value , put the installed reactor in the heating device, respectively collect the liquid temperature and steam temperature in the reactor; observe the liquid temperature and steam temperature changes, when the liquid temperature-time curve has a turning point and the separation trend from the steam temperature-time curve increases At this moment, read the liquid temperature value and the pressure value in the reactor, and the liquid temperature value is the complete evaporation temperature of the alcohol-based fuel under this pressure. The measuring device used for the measuring method disclosed by the invention comprises a reaction kettle and a heating device, and has simple operation, good airtightness and stable performance.

Description

technical field [0001] The invention relates to the field of energy fuels, in particular to a method and a device for measuring the complete evaporation temperature of alcohol-based fuels. Background technique [0002] Alcohol-based fuel is a complex mixed fuel that can be used as a gaseous fuel to replace natural gas in gas turbines. At normal temperature and pressure, the alcohol-based fuel is in a liquid state and needs to be gasified before it is injected into the gas turbine combustor for combustion. Therefore, it is necessary to know the complete evaporation temperature of the complex fuel under different pressures in the closed combustion system in advance in order to carry out the analysis of the fuel. Heating to vaporize. [0003] The laboratory often uses a comprehensive thermal analyzer (TG-DSC) to measure the evaporation temperature and latent heat of evaporation of the analyzed substance, and uses a pressurized thermogravimetric analyzer to test and analyze the...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N25/12
Inventor 肖云汉刘志坦阳绍军郝洪亮邵卫卫王凯王波王文飞张哲巅李玉刚常连成张涛朱鸿飞
Owner GUODIAN SCI & TECH RES INST