Concrete product surface frozen damage prevention material
A technology for concrete products and freezing damage, which is applied to the field of frost damage prevention materials on the surface of concrete products, can solve the problems of concrete performance deterioration, insufficient durability, freeze-thaw damage, etc., and achieves the effects of improving weather resistance, increasing service life, and strong permeability
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Embodiment 1
[0017] Preparation of materials for preventing freezing damage on the surface of 100kg concrete products:
[0018] a. According to the mass percentage, the viscosity is 20mm when the hydroxyl content is 8% and the temperature is 25°C 2 55.7kg of hydroxyl silicone oil per s, 5.0kg of γ-aminopropyltriethoxysilane, and 37.9kg of methyl tributanoximinosilane as a cross-linking agent were added to the reaction kettle in turn, and the stirring speed was 90 rpm At the same time, heat up the materials in the reactor, and when the temperature of the materials in the reactor reaches 45°C, open the vacuum valve, and start vacuuming in the reactor, the degree of vacuum is 0.096MPa, and the vacuuming time is 70 minutes;
[0019] b. Then add 0.5 kg of hexamethyldisilazane and 0.9 kg of dibutyltin dilaurate into the reaction kettle in turn, and continue to vacuumize for 40 minutes;
[0020] c. Finally, under the protection of nitrogen with a volume percentage of 99.99%, the product is seale...
Embodiment 2
[0022] Preparation of materials for preventing freezing damage on the surface of 100kg concrete products:
[0023] a. According to the mass percentage, the viscosity is 25mm when the hydroxyl content is 10% and the temperature is 25°C 2 / s Hydroxy silicone oil 55.4kg, γ-aminopropyltriethoxysilane 5.5kg, cross-linking agent vinyl tributylketoxime silane 37.5kg, add to the reaction kettle in turn, start stirring, stirring speed 100 rpm, At the same time, heat up the material in the reactor, and when the temperature of the material in the reactor reaches 55°C, open the vacuum valve, and start vacuuming in the reactor, the vacuum degree is 0.085MPa, and the vacuuming time is 90 minutes;
[0024] b. Then add 0.4 kg of hexamethyldisilazane and 1.2 kg of dibutyltin dilaurate into the reaction kettle in turn, and continue to vacuumize for 60 minutes;
[0025] c. Finally, under the protection of nitrogen with a volume percentage of 99.99%, the product is sealed and stored in cans to o...
Embodiment 3
[0027] 100kg concrete product surface freezing damage prevention material is prepared by the following method:
[0028] a. According to the mass percentage, the viscosity is 30mm when the hydroxyl content is 8% and the temperature is 25°C 2 / s Hydroxy silicone oil 55.1kg, γ-aminopropyltriethoxysilane 5.5kg, cross-linking agent is a mixture of methyl tributylketoxime silane 31.9kg and vinyl tributylketoxime silane 6.1kg and then added to the reaction After the kettle, start stirring, the stirring speed is 110 rpm, and at the same time, heat the materials in the reactor to raise the temperature. When the temperature of the materials in the reactor rises to 60°C, open the vacuum valve, and start vacuuming in the reactor. The vacuum degree is 0.096MPa. Vacuum time 50 minutes;
[0029] b. Then add 0.4 kg of hexamethyldisilazane and 1.0 kg of dibutyltin dilaurate into the reaction kettle in turn, and continue the vacuum reaction for 40 minutes;
[0030] c. Finally, under the prote...
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