Extrusion molding preparation method of gradient material in static magnetic field

A technology of extrusion molding and gradient materials, which is applied in the direction of magnetic properties of inorganic materials, can solve the problems of sudden changes in composition, complexity, and difficulty in achieving continuous and uniform changes in material components, and achieve the effects of simplified procedures and reduced costs

Inactive Publication Date: 2015-11-04
彭晓领
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, these preparation methods have important limitations
For example, powder molding is difficult to achieve continuous and uniform change of material components; vapor deposition is difficult to obtain large thickness materials; self-propagating combustion density is low; there are interfaces with sudden changes in composition between the plasma sprayed coatings; etc.
These methods require complex processes or equipment, and the lack of simple preparation methods is an important reason for limiting the further development of functionally graded materials.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] 1) Mud preparation

[0022] Combine strong magnetic metal Fe and weak magnetic ZrO in the mud refining machine 2 The ceramic mixed powder is added with organic solvent ethanol, dispersant herring oil and binder vinyl butyral, and uniformly mixed to obtain mud. The volume fraction of the organic solvent is 20% of the mud, the volume fraction of the dispersant is 0.2%, and the mass fraction of the adhesive is 10% of the mud;

[0023] 2) Extrusion molding in a static magnetic field

[0024] Extrude the mud in the extruder, the extrusion pressure is 0.2MPa, apply a static magnetic field at the extrusion port, and the magnetic field strength is 2T, and then obtain a green body;

[0025] 3) Drying and sintering

[0026] After drying at 20°C, sintering is carried out in a protective environment of argon at a sintering temperature of 1200°C, kept for 4 hours, and then cooled with the furnace.

Embodiment 2

[0028] 1) Mud preparation

[0029] Mix strong magnetic metal Co and weak magnetic SiC ceramic powder in a mud mill, add organic solvent methyl ethyl ketone, dispersant phosphate and binder polyvinyl alcohol, and mix uniformly to obtain mud. The volume fraction of the organic solvent is 30% of the mud, the volume fraction of the dispersant is 1%, and the mass fraction of the adhesive is 15% of the mud;

[0030] 2) Extrusion molding in a static magnetic field

[0031] Extrude the mud in the extruder, the extrusion pressure is 0.4MPa, apply a static magnetic field at the extrusion port, and the magnetic field strength is 1.2T, and then obtain a green body;

[0032] 3) Drying and sintering

[0033] After drying at 30°C, sintering is carried out in a nitrogen protective environment at a sintering temperature of 1300°C, kept for 4 hours, and then cooled with the furnace.

Embodiment 3

[0035] 1) Mud preparation

[0036] Strong magnetic metal Ni and weak magnetic Si 3 N 4 The ceramic mixed powder is added with organic solvent butanone, dispersant triolein and binder vinyl butyral, and uniformly mixed to obtain mud. The volume fraction of the organic solvent is 40% of the mud, the volume fraction of the dispersant is 2%, and the mass fraction of the adhesive is 20% of the mud;

[0037] 2) Extrusion molding in a static magnetic field

[0038] Extrude the mud in the extruder, the extrusion pressure is 0.5MPa, apply a static magnetic field at the extrusion port, and the magnetic field strength is 0.8T, and then obtain a green body;

[0039] 3) Drying and sintering

[0040] After drying at 40°C, sintering is carried out in a nitrogen protective environment at a sintering temperature of 1400°C, kept for 4 hours, and then cooled with the furnace.

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PUM

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Abstract

The invention discloses an extrusion molding preparation method of a gradient material in a static magnetic field. The method comprises the following steps: 1, adding an organic solvent, a dispersant and a binder into mixed power of strongly magnetic metal and weakly magnetic ceramics, and carrying out uniform mixing to obtain a mud material; 2, performing extrusion molding on the mud material in an extruder and accordingly obtaining a green compact, wherein the extrusion pressure is 0.2 to 0.8 MPa, a static magnetic field is applied to an extrusion port, and the magnetic field intensity is 0.01 to 2T; and 3, after dying is performed at a temperature of 20 to 80 DEG C, carrying out sintering, performing heat insulation for 4h, and then cooling in a furnace, wherein the sintering is carried out in an argon or nitrogen protection environment and the sintering temperature is 1200 to 1500 DEG C. The method provided by the invention has the following advantages: the gradient material with continuously changing components can be prepared; and by use of a mature extrusion forming technology, the procedures for producing the gradient material is simplified, the cost is decreased, and the performance is improved.

Description

technical field [0001] The invention relates to an extrusion molding preparation method of a gradient material in a static magnetic field, belonging to the field of material preparation. Background technique [0002] Extrusion molding refers to a processing method in which the material passes through the action between the extruder barrel and the screw, is heated and plasticized, pushed forward by the screw, and continuously passes through the machine head to make various cross-section products or semi-finished products. Traditional extrusion molding is used in the processing of thermoplastics and rubber. It can be used for batching, granulation, rubber filtration, etc., and can be used for continuous production to manufacture various continuous products such as pipes, profiles, plates (or sheets), films, Wire and cable coating, rubber tire tread strips, inner tube tubes, sealing strips, etc., have high production efficiency. With the development of technology, extrusion mo...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F3/20C22C1/05H01F1/09
Inventor 不公告发明人
Owner 彭晓领
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