Brazing filler metal for SiC base composite material connection
A technology of composite materials and brazing filler metals, applied in the direction of welding/cutting media/materials, welding equipment, welding media, etc.
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Embodiment approach 1
[0038] The present embodiment is the preparation of powdered solder, comprising the following steps:
[0039] (1) According to the composition 4wt% ~ 18wt% Ti or TiH 2 , 2wt% to 10wt% Al, and the rest is Cu. The powders of the three components are weighed, and the purity is higher than 99.0%;
[0040] (2) Put the weighed powder into a container filled with acetone for ultrasonic treatment to make the powder evenly mixed, and then dry at 60° C. to 80° C. to obtain solder powder.
Embodiment approach 2
[0042] The present embodiment is the preparation of powdered solder, comprising the following steps:
[0043] (1) According to the composition 4wt% ~ 18wt% Ti or TiH 2 , 2wt% to 10wt% Al, and the rest is Cu. The powders of the three components are weighed, and the purity is higher than 99.0%;
[0044] (2) Put the powder directly into an agate mortar and grind thoroughly, and mix evenly to obtain brazing material powder.
Embodiment approach 3
[0046] This embodiment is the preparation of paste solder, comprising the following steps:
[0047] (1) dissolving polyvinyl butyral (PVB) in cyclohexanone, so that the concentration is 1wt% to 8wt%, to obtain a uniform oily liquid as a binder;
[0048] (2) Evenly mix the binder with the solder powder obtained in Embodiment 1 or 2 to obtain a solder paste, wherein the additive amount of the binder is 45% to 80% of the weight of the solder.
[0049] Practical effect of solder
[0050] The solder has been used to study the joining of 3D needled C / SiC composites themselves and 3D braided C / SiC composites with niobium alloy (C-103) and metallic niobium. During the brazing process, the vacuum degree is 6×10 -3 Pa, the heating and cooling rate is 10°C / min, and the performance of the brazed joint is as follows.
[0051] (1) Self-connection of 3D needle-punched C / SiC composites
[0052] (1) The three-dimensional acupuncture C / SiC composite material (fiber volume fraction 27% ~ 28%...
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