Supercharge Your Innovation With Domain-Expert AI Agents!

Method used for determining puff-by-puff alkaloids in cigarette main stream smoke

A technology for mainstream cigarette smoke and alkaloids, which is applied in measuring devices, instruments, scientific instruments and other directions to achieve the effects of high efficiency, strong practicability and convenient testing

Inactive Publication Date: 2015-11-11
CHINA TOBACCO JIANGSU INDAL
View PDF6 Cites 1 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the content of alkaloids in the mainstream smoke of cigarettes is generally determined by stick, and the five alkaloids (nicotine, nornicotine, mesmin, pseudobasine and anonicotine) in the particulate matter of cigarette mainstream smoke are measured simultaneously. No studies on mouthful content have been reported

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Method used for determining puff-by-puff alkaloids in cigarette main stream smoke
  • Method used for determining puff-by-puff alkaloids in cigarette main stream smoke
  • Method used for determining puff-by-puff alkaloids in cigarette main stream smoke

Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0023] 1. Cigarette samples, main reagents and instruments used in this example

[0024] (1) Cigarette samples are shown in Table 1

[0025] Table 1 Cigarette samples and specifications (mg / stick)

[0026] cigarette sample box label tar box labeled nicotine box labeled carbon monoxide A 13 1.3 13 B 8 0.8 8 C 5 0.6 8 D 8 0.8 10 E 13 1.2 13

[0027] (2) Standard samples. Nicotine, nornicotine, mesmin, pseudobasine, anonicotine, 2,4'-bipyridine (internal standard), the above standard samples are chromatographically pure grade, purchased from Acros Organics Company in the United States, all standard samples Store in a refrigerator below 4°C for later use;

[0028] (3) Reagents. Ethyl acetate (chromatographically pure, SIGMA company), 5wt% sodium hydroxide solution, internal standard solution (2,4'-bipyridine with a concentration of 2000 μg / mL, using ethyl acetate as a solvent);

[0029] (4) Instruments. RM20 / CS turntable...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
diameteraaaaaaaaaa
Login to View More

Abstract

The invention discloses a method used for determining puff-by-puff alkaloids in cigarette main stream smoke. According to the method, an improved smoking machine is adopted; cigarettes to be tested are smoked successively; magnetic valves on a gas circuit are turned on respectively; particular matters in the smoke of the cigarettes to be tested are collected by total particular matter filter element collectors; filter elements are subjected to ultrasonic extraction and centrifugation, an obtained supernatant liquid is subjected to GC / MS analysis; and internal standard method quantitative analysis is carried out using five alkaloid standard samples. The improved smoking machine is provided with ten magnetic valves and ten total particular matter filter element collectors; smoking processes of the improved smoking machine is controlled by a control system; collection of the particular matters of each puff of twenty cigarettes is realized; the method high in repeatability and recovery rate when the method is used for determining alkaloids of particulates of smoke gas each puff; determination is convenient; efficiency is high; and practicality is high.

Description

technical field [0001] The invention belongs to the field of cigarette quality detection, and in particular relates to a method for measuring puff-by-puff alkaloids in mainstream smoke of cigarettes. Background technique [0002] Alkaloids are important components that affect the quality of tobacco leaves. In addition to nicotine, the main alkaloids in tobacco include nornicotine, mesmin, pseudobasine and neonicotinoid. Nicotine can directly stimulate the central nervous system of the human body and produce physiological reactions; nornicotine has a negative impact on the taste of cigarettes; mesmin has a mouse smell, which seriously affects the taste of cigarette products; alkali. Alkaloids are one of the direct precursors of tobacco-specific nitrosamines, which are easily metabolized into alkaloids in the process of tobacco preparation and cigarette smoking, and then form carcinogenic tobacco-specific nitrosamines with nitrite, especially The conversion of nicotine to no...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/02
Inventor 印德春薄云川丁超于海洋殷延齐严静郜明陶海涛李少鹏
Owner CHINA TOBACCO JIANGSU INDAL
Features
  • R&D
  • Intellectual Property
  • Life Sciences
  • Materials
  • Tech Scout
Why Patsnap Eureka
  • Unparalleled Data Quality
  • Higher Quality Content
  • 60% Fewer Hallucinations
Social media
Patsnap Eureka Blog
Learn More

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.

© 2025 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com