Method for utilizing gibberellins raffinate to prepare high-activity water flush fertilizer
A technology of gibberellin and raffinate, which is used in fertilization devices, applications, fertilizer mixtures, etc., to increase production, improve quality, and prevent pollution.
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Embodiment 1
[0042] Step 1: Preparation of gibberellin raffinate concentrate
[0043] Extract 5 t of gibberellin fermentation liquid through solvent extraction to separate gibberellin active components to obtain 2.2 t of gibberellin extraction waste liquid; remove residual organic solvents from the above gibberellin extraction waste liquid by atmospheric distillation and evaporate in a three-effect vacuum Concentrate, the concentration ratio is more than 10 times, and the prepared gibberellin raffinate concentrated solution with a specific gravity of 1.3g / mL is 200kg; wherein, the amino acid content in the gibberellin raffinate concentrated solution is 10.1%.
[0044] Step 2: Adjustment of the pH value of the gibberellin raffinate
[0045] In the reaction kettle, use 1mol / L NaOH solution to adjust the gibberellin raffinate concentrate to pH 7 to obtain neutral gibberellin raffinate; wherein, the amount of NaOH is according to the formula pH=0.0234×NaOH+2.566 calculate.
[0046] Step 3: P...
Embodiment 2
[0054] Step 1: Preparation of gibberellin raffinate concentrate
[0055] Extract 5 t of gibberellin fermentation liquid through solvent extraction to separate gibberellin active components to obtain 2.2 t of gibberellin extraction waste liquid; remove residual organic solvents from the above gibberellin extraction waste liquid by atmospheric distillation and evaporate in a three-effect vacuum Concentrate, the concentration ratio is more than 10 times, and the prepared gibberellin raffinate concentrated solution with a specific gravity of 1.3g / mL is 200kg; wherein, the amino acid content in the gibberellin raffinate concentrated solution is 10.1%.
[0056] Step 2: Adjustment of the pH value of the gibberellin raffinate
[0057] In the reaction kettle, use 1mol / L NaOH solution to adjust the gibberellin raffinate concentrate to pH 7 to obtain neutral gibberellin raffinate; wherein, the amount of NaOH is according to the formula pH=0.0234×NaOH+2.566 calculate.
[0058] Step 3: P...
Embodiment 3
[0066] Step 1: Preparation of gibberellin raffinate concentrate
[0067] Extract 5 t of gibberellin fermentation liquid through solvent extraction to separate gibberellin active components to obtain 2.2 t of gibberellin extraction waste liquid; remove residual organic solvents from the above gibberellin extraction waste liquid by atmospheric distillation and evaporate in a three-effect vacuum Concentrate, the concentration ratio is more than 10 times, and the prepared gibberellin raffinate concentrated solution with a specific gravity of 1.3g / mL is 200kg; wherein, the amino acid content in the gibberellin raffinate concentrated solution is 10.1%.
[0068] Step 2: Adjustment of the pH value of the gibberellin raffinate
[0069] In the reaction kettle, use 1mol / L NaOH solution to adjust the gibberellin raffinate concentrate to pH 7 to obtain neutral gibberellin raffinate; wherein, the amount of NaOH is according to the formula pH=0.0234×NaOH+2.566 calculate.
[0070] Step 3: P...
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