Preparation method of anti-bacterial and mite-proof sulfur-containing viscose fiber
A viscose fiber and anti-mite technology is applied in the field of preparation of antibacterial and anti-mite sulfur-containing viscose fibers, and can solve the problems of poor washability of surface coating method, high treatment cost of surface grafting method, low biological safety of functional materials, etc. problem, to solve the effect of poor fastness, low manufacturing cost and safe use
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example 1
[0017] Pre-prepared N-methylmorpholine-N-oxide (NMMO) spinning solvent with a water content of 10% at 85°C; then added 5% mass fraction of cellulose powder to the previously prepared spinning solvent , insulated and stirred at 95°C for 1 hour, the cellulose is fully dissolved, and made into a cellulose spinning solution; the temperature is quickly cooled to 30°C, and sublimated sulfur with a particle size of 300 mesh and a mass fraction of 5% is mixed in as an antibacterial and anti-mite functional component , blending and stirring to obtain a uniformly dispersed sulfur-containing cellulose spinning solution; water is used as the coagulation solution, and the spinning solution is extruded from the spinning orifice into the coagulation solution, and the spinning solution is gradually thinned during the rapid coagulation process. Viscose fiber, made of sulfur-containing viscose fiber with antibacterial and anti-mite functions.
[0018] The sublimated sulfur on the surface of thi...
example 2
[0020] Pre-prepared N-methylmorpholine-N-oxide (NMMO) spinning solvent with a water content of 12% at 90°C; then added 10% by mass of cellulose powder to the previously prepared spinning solvent , keep stirring at 90°C for 1.5 hours, the cellulose is fully dissolved, and made into a cellulose spinning solution; quickly cool down to 40°C, mix sublimated sulfur with a particle size of 400 mesh and a mass fraction of 10% as an antibacterial and anti-mite functional ingredient , blending and stirring to obtain a uniformly dispersed sulfur-containing cellulose spinning solution; water is used as the coagulation solution, and the spinning solution is extruded from the spinning orifice into the coagulation solution, and the spinning solution is gradually thinned during the rapid coagulation process. Viscose fiber, made of sulfur-containing viscose fiber with antibacterial and anti-mite functions.
[0021] The sublimated sulfur on the surface of this type of fiber can inhibit poisonou...
example 3
[0023] Pre-prepared N-methylmorpholine-N-oxide (NMMO) spinning solvent with a water content of 15% at 95°C; then added 20% mass fraction of cellulose powder to the previously prepared spinning solvent , insulated and stirred at 90°C for 3 hours, the cellulose was fully dissolved, and made into a cellulose spinning solution; the temperature was quickly cooled to 60°C, and sublimed sulfur with a particle size of 400 mesh and a mass fraction of 15% was mixed in as an antibacterial and anti-mite functional component , blending and stirring to obtain a uniformly dispersed sulfur-containing cellulose spinning solution; water is used as the coagulation solution, and the spinning solution is extruded from the spinning orifice into the coagulation solution, and the spinning solution is gradually thinned during the rapid coagulation process. Viscose fiber, made of sulfur-containing viscose fiber with antibacterial and anti-mite functions.
[0024] The sublimated sulfur on the surface of...
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