Natural antibacterial anti-aging rubber material and preparation method thereof
A rubber material and natural antibacterial technology, which is applied in the field of natural antibacterial and aging-resistant rubber materials and its preparation, can solve the problems of narrow antibacterial spectrum, single antibacterial component, easy failure, health and safety hazards, etc., to achieve complementary effects and improve mechanical properties.
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Embodiment 1
[0028] 1. Raw material preparation:
[0029] ①Preparation of plant source extracts: collect 21kg of rutabaga leaves, 52kg of walnut leaves, and 27kg of almond leaves in a fresh state, wash them separately, dry them, grind them into coarse powder and mix evenly, add 10 times the amount of coarse powder and decoct twice , 1.5h each time, filter, combine the filtrate and concentrate it to a solution with a relative density of 1.05 at 50°C, absorb it through D101 macroporous adsorption resin, elute with 8 times the column volume of 75wt% ethanol solution, collect the eluate under reduced pressure Concentrate and dry in vacuum to obtain the plant source extract;
[0030] ②Preparation of nano-loess: collect a certain amount of loess and put it into a muffle furnace, roast it at 350°C for 8 hours, and pulverize it into a 100-mesh fine powder after cooling. Stir and react at ℃ for 3 hours, add an appropriate amount of 25wt% sodium hydroxide solution to adjust the pH value to neutral,...
Embodiment 2
[0040] 1. Raw material preparation:
[0041] ①Preparation of plant-derived extracts: Collect 26kg of rutabaga leaves, 49kg of walnut leaves, and 25kg of almond leaves in a fresh state, wash them separately, dry them, grind them into coarse powder, mix well, add 15 times the amount of coarse powder and decoct twice , 2 hours each time, filter, combine the filtrate and concentrate to a solution with a relative density of 1.15 at 50°C, absorb it through D101 macroporous adsorption resin, elute with 6 times the column volume of 90wt% ethanol solution, collect the eluate and concentrate under reduced pressure , vacuum-dried to obtain plant-derived extracts;
[0042] ②Preparation of nano-loess: collect a certain amount of loess and send it into a muffle furnace, roast it at 250°C for 6h, and pulverize it into a 90-mesh fine powder after cooling. Stir and react at ℃ for 2 hours, add an appropriate amount of 25wt% sodium hydroxide solution to adjust the pH value to neutral, stir and ...
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