Photosensitive resin composition and uses thereof
A photosensitive resin and composition technology, applied in optics, optical filters, opto-mechanical equipment, etc., can solve the problems of unacceptable roughness in the industry and shrinkage of black matrix films.
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preparation example Construction
[0200] The preparation method of the photosensitive resin composition of the present invention is not particularly limited. For example, the black pigment (E) can be directly added into the photosensitive resin composition to disperse, or a part of the black pigment (E) can be dispersed in the In a part of the medium (medium) containing the alkali-soluble resin (A) and the solvent (D), after the pigment dispersion liquid is formed, it is combined with the compound (F) represented by the formula (a) and the compound (F) represented by the formula (b) having a fluorene skeleton The epoxy resin (G), the photoinitiator (C) and the rest of the solvent (D) are mixed and prepared. The dispersing step of the above-mentioned black pigment (E) can be performed by mixing the above-mentioned components with a mixer such as a bead mill or a roll mill.
[0201] The present invention also provides a black matrix formed from the aforementioned photosensitive resin composition.
[0202] The b...
Synthetic example 1
[0219] Synthesis example 1: Production method of resin (A-1-1) having an unsaturated group
[0220] With 100 parts by weight of fluorene epoxy compound (model ESF-300, manufactured by Nippon Steel Chemical; epoxy equivalent 231), 30 parts by weight of acrylic acid, 0.3 parts by weight of benzyltriethylammonium chloride, 0.1 parts by weight of 2,6-di-tert-butyl-p-cresol and 130 parts by weight of propylene glycol methyl ether acetate were continuously added to a 500mL four-necked flask, and the feeding rate was controlled at 25 parts by weight / minute, and the temperature was maintained at 100°C to Within the range of 110° C., after 15 hours of reaction, a light yellow transparent mixed liquid with a solid content concentration of 50 wt % can be obtained.
[0221] Then, 100 parts by weight of the above-mentioned mixed solution was dissolved in 25 parts by weight of ethylene glycol ether acetate, while adding 6 parts by weight of tetrahydrophthalic anhydride and 13 parts by weigh...
Synthetic example 2
[0222] Synthesis example 2: Manufacturing method of resin (A-1-2) having an unsaturated group
[0223] With 100 parts by weight of fluorene epoxy compound (model ESF-300, manufactured by Nippon Steel Chemical; epoxy equivalent 231), 30 parts by weight of acrylic acid, 0.3 parts by weight of benzyltriethylammonium chloride, 0.1 parts by weight of 2,6-di-tert-butyl-p-cresol and 130 parts by weight of propylene glycol methyl ether acetate were continuously added to a 500mL four-necked flask, and the feeding rate was controlled at 25 parts by weight / minute, and the temperature was maintained at 100°C to Within the range of 110° C., after 15 hours of reaction, a light yellow transparent mixed liquid with a solid content concentration of 50 wt % can be obtained.
[0224] Next, 100 parts by weight of the above mixed solution was dissolved in 25 parts by weight of ethylene glycol ether acetate, and 13 parts by weight of benzophenone tetracarboxylic dianhydride was added at the same ti...
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Abstract
Description
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