Ninhydrin/nanometer titanium dioxide compound and preparing method and application thereof

A nano-titanium dioxide and ninhydrin technology is applied in the direction of chemical reaction of materials for analysis, and material analysis by observing the impact on chemical indicators. It can solve the problems of easy diffusion of spots and complicated operations, and achieve rich sources. , low price and easy availability, the effect of reducing the time required for color development

Active Publication Date: 2016-01-27
ZHEJIANG FORESTRY UNIVERSITY
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The complex is incorporated into the stationary phase of the thin-layer chromatography plate to prepare a new type of thin-layer chromatography plate, which realizes the on

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  • Ninhydrin/nanometer titanium dioxide compound and preparing method and application thereof
  • Ninhydrin/nanometer titanium dioxide compound and preparing method and application thereof
  • Ninhydrin/nanometer titanium dioxide compound and preparing method and application thereof

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Embodiment Construction

[0035] The present invention will be further described below in combination with specific embodiments and accompanying drawings.

[0036] 1. Preparation of ninhydrin / nano-titanium dioxide composite

[0037] (1) Prepare a 100 mM tetrabutyl titanate solution, the solvent is a toluene / ethanol solution (v:v=1:1), and stir at room temperature for one hour.

[0038] (2) Put flexible fiber paper, which can also be one of face tissue and quantitative filter paper, in a suction filtration device, rinse it with ethanol for 2-3 times, remove the moisture therein, and dry it with air flow. Pipette about 10 mL of tetrabutyl titanate solution into the suction filtration device, and let stand for 3 minutes, so that the tetrabutyl titanate solution is fully soaked in the cellulose paper.

[0039] (3) Turn on the suction filtration device to slowly filter the tetrabutyl titanate solution through the cellulose paper, then add ethanol for 2-3 rinses, and let stand for 2 minutes.

[0040] (4) R...

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Abstract

The invention discloses a ninhydrin/nanometer titanium dioxide compound and a preparing method and application thereof. The preparing method comprises the steps that 1, a polymeric precursor solution is prepared; 2, suction filtration is utilized for enabling the polymeric precursor solution to pass through a dehydrated filter membrane, and the filter membrane can adsorb the polymeric precursor solution in a saturated mode; 3, suction filtration is utilized for enabling a ninhydrin solution to pass through the filter membrane to react to generate the ninhydrin/nanometer titanium dioxide compound. The compound has good developing sensitivity to amino acid and can serve as a color developing agent for a thin layer chromatography plate to detect amino acid. The invention further discloses a thin layer chromatography plate which comprises a base material and a stationary phase. The stationary phase contains the ninhydrin/nanometer titanium dioxide compound. The compound is doped into the stationary phase of the thin layer chromatography plate to prepare the novel thin layer chromatography plate. By the utilization of the thin layer chromatography plate, chromatographic separation and color development processes are completed through one step, and use is convenient.

Description

technical field [0001] The invention relates to the field of food detection and analysis, in particular to a ninhydrin / nano-titanium dioxide composite and its preparation method and application. Background technique [0002] Thin layer analysis is one of the commonly used methods in the analysis of amino acids, lipids, drugs and other substances. Amino acid is a common amphoteric compound, and chromatography is the most effective method for its separation and identification. Although there are currently highly automated amino acid analysis instruments for sale, thin-layer chromatography is still widely used in ordinary laboratories or factories and mines because of its economical, convenient and quick advantages. Spread the stationary phase (also called adsorbent) evenly on the carrier to form a thin layer, point the sample to be analyzed on one end of the thin layer plate, and then immerse the sample point in a suitable developing agent, in a closed chromatography Chromat...

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Application Information

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IPC IPC(8): G01N21/78
Inventor 张宜明叶海鹏李顺黄建国胡良刘兴泉冯震吴俊樊凯
Owner ZHEJIANG FORESTRY UNIVERSITY
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