A kind of polyvinyl alcohol modified antimony trioxide and preparation method thereof
A technology of antimony trioxide and polyvinyl alcohol, which is applied in the treatment of dyed polymer organic compounds, fibrous fillers, etc., can solve the problems of high specific gravity, poor dispersion and easy settlement of flame retardant antimony trioxide, and achieve Good similar miscibility, small intermolecular distance, and enhanced mechanical riveting effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0033] Add antimony trioxide powder with a particle diameter of 0.5-5 μm into distilled water, and change mechanical stirring while adding the powder to prepare a 30% antimony trioxide slurry. Put the antimony trioxide slurry into the ultrasonic generator, the ultrasonic power is 200-600W, the working frequency is 20-40kHz, and the ultrasonic wave is irradiated for 15 minutes. Add polyvinyl alcohol into the container, then add distilled water, and heat and stir at 90° C. for 20 min to prepare a 10% polyvinyl alcohol solution. In the container, first add the polyvinyl alcohol solution, and then add the pretreated antimony trioxide slurry, the mass ratio is 3:100, and the dry basis ratio is 1:100. Then, under the condition of 100° C., high-speed stirring and reacting for 20 minutes, an active antimony trioxide water-based suspension was prepared, and the mass concentration of the antimony trioxide suspension was about 30%. Weigh a certain amount of active antimony trioxide wate...
Embodiment 2
[0035] Add antimony trioxide powder with a particle diameter of 0.5-5 μm into distilled water, and change mechanical stirring while adding the powder to prepare a 40% antimony trioxide slurry. Put the antimony trioxide slurry into the ultrasonic generator, the ultrasonic power is 200-600W, the working frequency is 20-40kHz, and the ultrasonic wave is irradiated for 30min. Add polyvinyl alcohol into the container, then add distilled water, and heat and stir at 90° C. for 30 min to prepare a 10% polyvinyl alcohol solution. In the container, the polyvinyl alcohol solution is added first, and then the pretreated antimony trioxide slurry is added, the mass ratio is 20:100, and the dry basis ratio is 5:100. Then, under the condition of 60° C., high-speed stirring and reacting for 40 minutes, the polyvinyl alcohol modified antimony trioxide water-based suspension was prepared, and the mass concentration of the antimony trioxide suspension was 35%. Weigh a certain amount of active an...
Embodiment 3
[0037]Add antimony trioxide powder with a particle diameter of 0.5-5 μm into distilled water, and change mechanical stirring while adding the powder to prepare a 25% antimony trioxide slurry. Put the antimony trioxide slurry into a shear emulsification tester at a speed of 3000r / min, and shear and stir for 15min. Add polyvinyl alcohol into the container, then add distilled water, and heat and stir at 90° C. for 40 min to prepare a 10% polyvinyl alcohol solution. In the container, first add the polyvinyl alcohol solution, and then add the pretreated antimony trioxide slurry, the mass ratio is 7.5:100, and the dry basis ratio is 3:100. Then, under the condition of 90° C., high-speed stirring and reacting for 30 minutes, the polyvinyl alcohol-modified antimony trioxide water-based suspension was prepared, and the mass concentration of the antimony trioxide suspension was about 24%. Weigh a certain amount of active antimony trioxide water-based suspension, and then add dropwise 0...
PUM
| Property | Measurement | Unit |
|---|---|---|
| particle diameter | aaaaa | aaaaa |
| particle diameter | aaaaa | aaaaa |
| particle diameter | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
Login to View More