Low-temperature environment-friendly conductive silver paste and preparation method and application thereof
A conductive silver paste, environmental protection technology, applied in cable/conductor manufacturing, conductive materials dispersed in non-conductive inorganic materials, circuits, etc., can solve the problems of poor conductivity, poor adhesion between conductive silver paste and substrate, etc. Achieve high conductivity, easy control of process conditions, and high adhesion
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[0030] Correspondingly, on the basis of the low-temperature environment-friendly conductive silver paste described above, the embodiment of the present invention also provides a preparation method of the low-temperature environment-friendly conductive silver paste according to the embodiment of the present invention. In one embodiment, the preparation method of the low-temperature environment-friendly conductive silver paste comprises the following steps:
[0031] S01: Weigh each component according to the components contained in the low-temperature environment-friendly conductive silver paste of the present invention;
[0032] S02: performing a first mixing treatment on the weighed organic carrier and the flake silver powder to prepare a first mixture;
[0033] S03: performing a second mixing treatment on the weighed ultra-fine silver and the first mixture to prepare a second mixture;
[0034] S04: performing a third mixing treatment on the weighed additive and the second mi...
Embodiment 1
[0045] This embodiment provides a low-temperature environment-friendly conductive silver paste, which is composed of an organic carrier, flake silver powder, ultrafine silver powder, silane coupling agent and putty powder.
[0046] Its preparation method is as follows:
[0047] S11: Dissolve 10 g of polyester resin into 45 g of propylene glycol methyl ether acetate, heat and stir at a constant temperature at 60° C. until completely dissolved, filter and cool to obtain an organic carrier;
[0048] S12: Weigh 55g of flaky silver powder with an average size of 2 μm and dissolve it into the aforementioned 28g of organic carrier, stir thoroughly with a mixer until the mixture is evenly mixed to obtain a silver powder mixture (1); weigh 25g of ultrafine silver powder with an average particle size of 20nm and add it to the In the silver powder mixture (1), fully stir with a mixer until the mixture is evenly mixed to obtain the silver powder mixture (2).
[0049] S13: Weigh 0.2g of s...
Embodiment 2
[0053] This embodiment provides a low-temperature environment-friendly conductive silver paste, which is composed of an organic carrier, flake silver powder, ultrafine silver powder, silane coupling agent and putty powder.
[0054] Its preparation method is as follows:
[0055] S21: Weigh 10 g of polyester resin and dissolve it in 35 g of ethylene glycol ether acetate solvent, heat and stir at a constant temperature at 60° C. until completely dissolved, filter and cool to obtain an organic vehicle.
[0056] S22: Weigh 48g of flaky silver powder with an average size of 2 μm and dissolve it into the aforementioned 32g of organic carrier, stir fully with a mixer until mixed to obtain a silver powder mixture (1); weigh 18g of ultrafine silver powder with an average particle size of 20nm and add it to the In the silver powder mixture (1), fully stir with a mixer until the mixture is evenly mixed to obtain the silver powder mixture (2).
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Abstract
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