A kind of high-strength magnesium alloy and preparation method thereof
A technology of magnesium alloy and manufacturing method, which is applied in the field of nano-additive reinforced magnesium alloy and its preparation, can solve problems such as strength gap, achieve the effect of increasing strength, strengthening effect, and improving plasticity of alloy
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Embodiment 1
[0029] (1) Prepare raw materials: prepare more than 99.9% high-purity magnesium and high-purity aluminum, and nano-SiO with an average particle size of 80 nanometers 2 ;
[0030] (2) Smelting alloy: The high-purity magnesium and zinc are batched according to the atomic ratio of 3:1. 2 Smelting in mixed gas with SF6, in which CO 2 The volume ratio to SF6 is 100:1; nano-SiO, which accounts for 4.2% of the alloy mass fraction, is added during the smelting process 2 , keep the temperature at 700 ° C, and disperse by ultrasonic method;
[0031] (3) Slowly cool the alloy ingot, the cooling rate is 0.2k per second; keep the vacuum state during the cooling process, the vacuum degree is 4torr;
[0032] (4) After cooling, the alloy ingot is processed into a disc shape;
[0033] (5) Put the coarse-grained alloy disc processed in step (4) into the space formed by the grooves in the upper and lower anvils, apply a high pressure of 4.5GPa to the alloy, and rotate the pressure at a speed...
Embodiment 2
[0035] (1) Prepare raw materials: prepare more than 99.9% high-purity magnesium and high-purity zinc, and nano-SiC with an average particle size of 90 nanometers;
[0036] (2) Smelting alloy: The high-purity magnesium and zinc are batched according to the atomic ratio of 6:1. 2 Smelting in mixed gas with SF6, in which CO 2 The volume ratio to SF6 is 80:1; during the smelting process, nano-SiC, which accounts for 1.5% of the alloy mass fraction, is added, the temperature is kept at 700 °C, and the ultrasonic method is used for dispersion;
[0037] (3) Slowly cool the alloy ingot, the cooling rate is 0.3k per second; keep the vacuum state during the cooling process, the vacuum degree is 3torr;
[0038] (4) After cooling, the alloy ingot is processed into a disc shape;
[0039] (5) Put the coarse-grained alloy disc processed in step (4) into the space formed by the grooves in the upper and lower anvils, apply a high pressure of 5GPa to the alloy, and rotate the anvil at a speed o...
Embodiment 3
[0041] (1) Prepare raw materials: prepare more than 99.9% high-purity magnesium and high-purity zinc, and nano-SiC with an average particle size of 60 nanometers;
[0042] (2) Smelting alloy: The high-purity magnesium and zinc are batched according to the atomic ratio of 3.5:1. 2 Smelting in mixed gas with SF6, in which CO 2 The volume ratio to SF6 is 50:1; during the smelting process, nano-SiC, which accounts for 1.8% of the alloy mass fraction, is added, the temperature is kept at 700 °C, and the ultrasonic method is used to disperse;
[0043] (3) Slowly cool the alloy ingot, the cooling rate is 0.5k per second; keep the vacuum state during the cooling process, the vacuum degree is 3torr;
[0044] (4) After cooling, the alloy ingot is processed into a disc shape;
[0045] (5) Put the coarse-grained alloy disc processed in step (4) into the space formed by the grooves in the upper and lower anvils, apply a high pressure of 1.5GPa to the alloy, and rotate the pressure at a s...
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