Rush medulla junci modification-based 3D printer base material and preparation method thereof

A technology of 3D printers and rushes, which is applied in the base material of 3D printers modified based on rushes and its preparation field, which can solve the problems of high cost of metal bases, poor mechanical properties of polymer bases in terms of anti-aging, affecting the application of polymer bases, etc. question

Inactive Publication Date: 2016-04-06
ANHUI CHUNGU 3D PRINTING INTELLIGENT EQUIP IND TECH RES INST CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although the metal base has strong mechanical properties, the cost of the metal base is high
Although the cost of the polymer base is relatively cheap,

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0012] The invention provides a method for preparing a 3D printer base material modified based on rushes, comprising:

[0013] 1) Finishing and crushing the rush grass, then mixing the rush grass powder and bamboo charcoal powder and soaking in the mixed solution of 1-naphthylamine and hydrochloric acid, and then filtering to take the filter cake to obtain a modified composition;

[0014] 2) Combine expanded polystyrene, modified composition, polyacrylonitrile, polychlorotrifluoroethylene, silicon dioxide, 2-mercaptophenylthiazole, dilauryl thiodipropionate, steel fiber, mica Powder, dioctyl adipate and zinc borate are mixed, then melted, cooled and pelletized to make the base material for 3D printers.

[0015] In the step 1) of the present invention, the specific conditions for finishing can be selected in a wide range, but in order to make the prepared 3D printer base material have more excellent mechanical properties and oxidation resistance, preferably, in step 1) , at le...

Embodiment 1

[0027] 1) The rushes were killed at 155°C for 30 minutes, crushed to a particle size of 0.2mm, and then the rushes powder, bamboo charcoal powder (particle size: 0.3mm), 1-naphthylamine, hydrochloric acid (mass fraction: 24%) According to the weight ratio of 100:30:35:130, mix and soak at 75°C for 2.5 hours, then filter and take the filter cake to obtain the modified composition;

[0028] 2) Expanded polystyrene (weight average molecular weight is 4500), modified composition (weight average molecular weight is 5000), polyacrylonitrile (weight average molecular weight is 10000), polychlorotrifluoroethylene, silicon dioxide, 2 - Mercaptophenylthiazole, dilauryl thiodipropionate, steel fibers (length 3 mm, diameter 0.2 mm in radial section), mica powder, dioctyl adipate and zinc borate according to 100: Mix at a weight ratio of 16:60:35:15:12:45:20:15:20:15, then melt at 185°C for 35min, cool at 25°C and granulate to prepare 3D printer base material A1.

Embodiment 2

[0030] 1) The rushes were killed at 145°C for 25 minutes, crushed to a particle size of 0.1mm, and then the rushes powder, bamboo charcoal powder (particle size: 0.2mm), 1-naphthylamine, hydrochloric acid (mass fraction: 20%) According to the weight ratio of 100:27:30:120, mix and soak at 70°C for 2 hours, then filter and take the filter cake to obtain the modified composition;

[0031] 2) Expanded polystyrene (weight-average molecular weight is 3500), modified composition (weight-average molecular weight is 4000), polyacrylonitrile (weight-average molecular weight is 8000), polychlorotrifluoroethylene, silicon dioxide, 2 - Mercaptophenylthiazole, dilauryl thiodipropionate, steel fibers (length 1 mm, diameter 0.1 mm in radial section), mica powder, dioctyl adipate and zinc borate according to 100: 14:56:33:10:9:40:14:8:12:7 were mixed at a weight ratio, then melted at 180°C for 30 minutes, cooled at 15°C and granulated to prepare 3D printer base material A2.

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Abstract

The invention discloses a rush medulla junci modification-based 3D printer base material and a preparation method thereof. The preparation method comprises the following steps: (1) performing fixation and smashing on rush medulla junci, then mixing rush medulla junci powder with bamboo charcoal powder and soaking into a mixed solution of 1-naphthylamine and hydrochloric acid, and then filtering to take a filter cake to prepare a modified composition; (2) mixing expanded polystyrene, the modified composition, polyacrylonitrile, polychloro trifluoroethylene, silica, 2-sulfhydryl phenylthiazole, dilauryl thiodipropionate, steel fibers, mica powder, dioctyl adipate and zinc borate, and then fusing, cooling and pelleting to prepare the 3D printer base material. The 3D printer base material prepared through the method has excellent shock resistance and ageing resistance.

Description

technical field [0001] The invention relates to a base material for a 3D printer, in particular to a modified rush-based base material for a 3D printer and a preparation method thereof. Background technique [0002] The 3D printer base is one of the more important components in the 3D printer. The 3D printer base only needs to play the role of support and load-bearing. In actual production, the requirement for the 3D printer base is to have excellent stability and mechanical properties. [0003] At present, the 3D printer base can be divided into metal base and polymer base according to the material. Although the metal base has strong mechanical properties, the cost of the metal base is high. Although the cost of the polymer base is relatively cheap, the mechanical properties and anti-aging aspects of the polymer base are poor, which greatly affects the application of the polymer base in 3D printers. Contents of the invention [0004] The purpose of the present inventio...

Claims

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Application Information

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IPC IPC(8): C08L25/06C08L97/02C08L33/20C08L27/12C08K13/04C08K3/36C08K5/47C08K7/06C08K5/11C08K3/38
CPCC08L25/06C08L2203/14C08L2205/035
Inventor 宗泽吕月林吕晨黄仲佳郑兰斌吴志华刘俊松
Owner ANHUI CHUNGU 3D PRINTING INTELLIGENT EQUIP IND TECH RES INST CO LTD
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